(5-bromo-2,3-dichlorobenzyloxy)(tert-butyl)dimethylsilane

Base Information

Chemical Name:(5-bromo-2,3-dichlorobenzyloxy)(tert-butyl)dimethylsilane
CAS No.:1229245-67-3
Molecular Formula:C₁₃H₁₉BrCl₂OSi
Molecular Weight:370.189
Hs Code.:
Mol file:1229245-67-3.mol

Synonyms:(5-bromo-2,3-dichlorobenzyloxy)(tert-butyl)dimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5-bromo-2,3-dichlorobenzyloxy)(tert-butyl)dimethylsilane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (5-bromo-2,3-dichlorobenzyloxy)(tert-butyl)dimethylsilane

There total 3 articles about (5-bromo-2,3-dichlorobenzyloxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229245-68-4
(5-bromo-2,3-dichlorophenyl)methanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1229245-67-3
{[(5-bromo-2,3-dichlorophenyl)methyl]oxy}(1,1-dimethylethyl)dimethylsilane

Guidance literature:: With 1H-imidazole; at 20 ℃; for 16h;

Reference yield:

: 1229246-37-0
5-bromo-2,3-dichlorobenzaldehyde

: 1229245-67-3
{[(5-bromo-2,3-dichlorophenyl)methyl]oxy}(1,1-dimethylethyl)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / tetrahydrofuran; methanol / 2.75 h / 0 °C

2: 1H-imidazole / 16 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; In tetrahydrofuran; methanol;

Reference yield:

: 6334-18-5
2,3-dichlorobenzylaldehyde

: 1229245-67-3
{[(5-bromo-2,3-dichlorophenyl)methyl]oxy}(1,1-dimethylethyl)dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; sulfuric acid; trifluoroacetic acid / 75 h / 20 °C

2: sodium tetrahydroborate / tetrahydrofuran; methanol / 2.75 h / 0 °C

3: 1H-imidazole / 16 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; N-Bromosuccinimide; sulfuric acid; trifluoroacetic acid; In tetrahydrofuran; methanol;