Technology Process of 2-FLUORO,3-BROMO BENZALDOXIME
There total 3 articles about 2-FLUORO,3-BROMO BENZALDOXIME which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide; hydroxylamine hydrochloride;
In
tetrahydrofuran; methanol; water;
at 20 ℃;
for 16h;
pH=9;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 12.08 h
1.2: 2 h
2.1: pyridinium chlorochromate / dichloromethane / 1.08 h / Molecular sieve
3.1: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9
With
potassium hydroxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium chlorochromate / dichloromethane / 1.08 h / Molecular sieve
2: potassium hydroxide; hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 16 h / 20 °C / pH 9
With
potassium hydroxide; hydroxylamine hydrochloride; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; dichloromethane; water;
