4-BroMo-1-fluoro-2-isopropoxybenzene

Base Information

• Chemical Name: 4-BroMo-1-fluoro-2-isopropoxybenzene
• CAS No.: 944278-95-9
• Molecular Formula: C9H10BrFO
• Molecular Weight: 233.08
• Hs Code.: 2909309090
• Mol file: 944278-95-9.mol

Synonyms:4-BroMo-1-fluoro-2-isopropoxybenzene;4-Bromo-1-fluoro-2-(1-methylethoxy)-benzene

Chemical Property of 4-BroMo-1-fluoro-2-isopropoxybenzene

Chemical Property:

• PSA: 9.23000
• LogP: 3.37540

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-1-fluoro-2-isopropoxybenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-BroMo-1-fluoro-2-isopropoxybenzene

There total 2 articles about 4-BroMo-1-fluoro-2-isopropoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

isopropyl bromide (75-26-3) + 5-Bromo-2-fluorophenol (112204-58-7) → 5-bromo-2-fluoro-1-(isopropyloxy)benzene (944278-95-9)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 22h;

Reference yield: 86.0%

2-iodo-propane (75-30-9) + 5-Bromo-2-fluorophenol (112204-58-7) → 5-bromo-2-fluoro-1-(isopropyloxy)benzene (944278-95-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃;

Reference yield: 23.0%

5-bromo-2-fluoro-1-(isopropyloxy)benzene (944278-95-9) + oxalic acid diethyl ester (95-92-1) → ethyl 2-[4-fluoro-3-(isopropyloxy)phenyl]-2-oxoacetate

Guidance literature:

5-bromo-2-fluoro-1-(isopropyloxy)benzene; With iodine; magnesium; In tetrahydrofuran; at 40 ℃; Inert atmosphere;

oxalic acid diethyl ester; In tetrahydrofuran; at -50 - 20 ℃; for 18h; Inert atmosphere;

upstream raw materials:

2-iodo-propane

5-Bromo-2-fluorophenol

isopropyl bromide

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