Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrabroMo-

Base Information

• Chemical Name: Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrabroMo-
• CAS No.: 7314-86-5
• Molecular Formula: C10H12Br4
• Molecular Weight: 451.821
• Mol file: 7314-86-5.mol

Synonyms:Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrabroMo-

Chemical Property of Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrabroMo-

Chemical Property:

• Melting Point: 246-247 °C
• Boiling Point: 365.6±37.0 °C(Predicted)
• PSA: 0.00000
• Density: 2.568±0.06 g/cm3(Predicted)
• LogP: 4.90260
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

≥99% ^*data from raw suppliers

1,3,5,7-Tetrabromoadamantane 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrabroMo-

There total 7 articles about Tricyclo[3.3.1.13,7]decane, 1,3,5,7-tetrabroMo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,3,5-tribromoadamantane (707-34-6) → 1,3,5,7-tetrabromoadamantane (7314-86-5)

Guidance literature:

With aluminum tri-bromide; bromine; 1) 12 h, r.t., 2) 24 h, 150 deg C;

Reference yield: 94.0%

adamantane (281-23-2) → 1,3,5,7-tetrabromoadamantane (7314-86-5)

Guidance literature:

With aluminium trichloride; bromine; for 9h; Heating;

DOI:10.1021/ol036526g

Reference yield:

1-Adamantyl bromide (768-90-1) → 1,3,5,7-tetrabromoadamantane (7314-86-5)

Guidance literature:

Multi-step reaction with 2 steps

1: dibutyl ether; diethyl ether / 105 °C / Schlenk technique; Inert atmosphere

2: bromine; aluminum tri-bromide / 0 - 70 °C

With aluminum tri-bromide; bromine; In diethyl ether; dibutyl ether;

DOI:10.1002/ejoc.202101004

upstream raw materials:

1,3,5-tribromoadamantane

adamantane

1-Adamantyl bromide

Downstream raw materials:

1,3,5,7-tetrakis(phenyl)adamantane

1,3,5,7-tetranitroadamantane

1,3,5,7-Tetracyclohexyl-adamantan

1,3,5,7-tetrakis(4-methoxyphenyl)adamantane