Benzoic acid, 2-[(3,5,6-trimethyl-2-pyrazinyl)methoxy]-, ethyl ester

Base Information

Chemical Name:Benzoic acid, 2-[(3,5,6-trimethyl-2-pyrazinyl)methoxy]-, ethyl ester
CAS No.:947243-90-5
Molecular Formula:C17H20N2O3
Molecular Weight:0
Hs Code.:
Mol file:947243-90-5.mol

Synonyms:Benzoic acid, 2-[(3,5,6-trimethyl-2-pyrazinyl)methoxy]-, ethyl ester

Suppliers and Price of Benzoic acid, 2-[(3,5,6-trimethyl-2-pyrazinyl)methoxy]-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of Benzoic acid, 2-[(3,5,6-trimethyl-2-pyrazinyl)methoxy]-, ethyl ester

Chemical Property:

Melting Point:64 - 68 °C (hexane)
PSA：61.31000
LogP:3.15750

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of Benzoic acid, 2-[(3,5,6-trimethyl-2-pyrazinyl)methoxy]-, ethyl ester

There total 3 articles about Benzoic acid, 2-[(3,5,6-trimethyl-2-pyrazinyl)methoxy]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 123624-90-8
2-(chloromethyl)-3,5,6-trimethylpyrazine

: 118-61-6
2-hydroxy-benzoic acid ethyl ester

: 947243-90-5
ethyl 2-[(3,5,6-trimethylpyrazin-2-yl)methoxy]benzoate

Guidance literature:: 2-hydroxy-benzoic acid ethyl ester; With tetrabutylammomium bromide; potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 0.166667h;

2-(chloromethyl)-3,5,6-trimethylpyrazine; In N,N-dimethyl-formamide; at 60 ℃; for 6h;
DOI:10.1039/c3md20352b

Reference yield: 50.0%

: 79074-45-6
2-(bromomethyl)-3,5,6-trimethylpyrazine

: 118-61-6
2-hydroxy-benzoic acid ethyl ester

: 947243-90-5
ethyl 2-[(3,5,6-trimethylpyrazin-2-yl)methoxy]benzoate

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 2h;
DOI:10.1002/cbdv.200900353

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 947243-90-5
ethyl 2-[(3,5,6-trimethylpyrazin-2-yl)methoxy]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / 24 h / Reflux

2.1: potassium carbonate; tetrabutylammomium bromide / N,N-dimethyl-formamide / 0.17 h / 25 °C

2.2: 6 h / 60 °C

With thionyl chloride; tetrabutylammomium bromide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/c3md20352b