2-N,N-DIMETHYLAMINO-6-IODOPYRAZINE

Base Information

• Chemical Name: 2-N,N-DIMETHYLAMINO-6-IODOPYRAZINE
• CAS No.: 125060-66-4
• Molecular Formula: C6H8IN3
• Molecular Weight: 249.054
• Hs Code.: 2933990090
• Mol file: 125060-66-4.mol

Synonyms:2-N,N-DIMETHYLAMINO-6-IODOPYRAZINE;6-iodo-N,N-dimethyl-2-Pyrazinamine

Chemical Property of 2-N,N-DIMETHYLAMINO-6-IODOPYRAZINE

Chemical Property:

• Vapor Pressure: 0.00123mmHg at 25°C
• Boiling Point: 298.9°C at 760 mmHg
• PKA: 1.24±0.10(Predicted)
• Flash Point: 134.6°C
• PSA: 29.02000
• Density: 1.831g/cm³
• LogP: 1.14720

Purity/Quality:

98%Min ^*data from raw suppliers

2-(N,N-Dimethylamino)-6-iodopyrazine ^*data from reagent suppliers

Safty Information:

• Statements: 43
• Safety Statements: 36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-N,N-DIMETHYLAMINO-6-IODOPYRAZINE

There total 2 articles about 2-N,N-DIMETHYLAMINO-6-IODOPYRAZINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2,6-diiodopyrazine (58138-79-7) + dimethyl amine (124-40-3) → 2-iodo-6-(dimethylamino)pyrazine (125060-66-4)

Guidance literature:

In methanol; water; for 1h; Heating;

DOI:10.1021/jm00080a014

Reference yield:

2,6-diiodopyrazine (58138-79-7) → 2-iodo-6-(dimethylamino)pyrazine (125060-66-4)

Guidance literature:

With dimethyl amine; In methanol;

Reference yield:

1-azabicyclo[2.2.1]heptan-3-one (21472-89-9) + 2-iodo-6-(dimethylamino)pyrazine (125060-66-4) → (3S,4S)-3-(6-Dimethylamino-pyrazin-2-yl)-1-aza-bicyclo[2.2.1]heptan-3-ol (125059-73-6,125085-89-4)

Guidance literature:

With tert.-butyl lithium; Multistep reaction; 1.) pentane, Et₂O, - 50 deg C, 0.25 h, 2.) pentane, Et₂O, RT, 2 h;

DOI:10.1021/jm00080a014

upstream raw materials:

2,6-diiodopyrazine

dimethyl amine

Downstream raw materials:

(3S,4S)-3-(6-Dimethylamino-pyrazin-2-yl)-1-aza-bicyclo[2.2.1]heptan-3-ol

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