3-(4-Chlorophenyl)-4-ethyl-5-(methylthio)-4H-1,2,4-triazole

Base Information

Chemical Name:3-(4-Chlorophenyl)-4-ethyl-5-(methylthio)-4H-1,2,4-triazole
CAS No.:31409-18-4
Molecular Formula:C11H12 Cl N3 S
Molecular Weight:253.75
Hs Code.:2933990090
Mol file:31409-18-4.mol

Synonyms:4H-1,2,4-Triazole,3-(p-chlorophenyl)-4-ethyl-5-(methylthio)- (8CI)

Suppliers and Price of 3-(4-Chlorophenyl)-4-ethyl-5-(methylthio)-4H-1,2,4-triazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-(4-CHLOROPHENYL)-4-ETHYL-5-(METHYLTHIO)-4H-1,2,4-TRIAZOLE 95.00%
5MG
$ 498.81

Total 3 raw suppliers

Chemical Property of 3-(4-Chlorophenyl)-4-ethyl-5-(methylthio)-4H-1,2,4-triazole

Chemical Property:

Vapor Pressure:2.74E-07mmHg at 25°C
Melting Point:113-115 °C
Boiling Point:420.8°Cat760mmHg
PKA:1.33±0.10(Predicted)
Flash Point:208.3°C
PSA：56.01000
Density:1.3g/cm³
LogP:3.34030

Purity/Quality:

99% ^*data from raw suppliers

3-(4-CHLOROPHENYL)-4-ETHYL-5-(METHYLTHIO)-4H-1,2,4-TRIAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(4-Chlorophenyl)-4-ethyl-5-(methylthio)-4H-1,2,4-triazole

There total 4 articles about 3-(4-Chlorophenyl)-4-ethyl-5-(methylthio)-4H-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 26131-64-6
5-(4-Chloro-phenyl)-4-ethyl-2,4-dihydro-[1,2,4]triazole-3-thione

: 74-88-4
methyl iodide

: 31409-18-4
3-(4-chloro-phenyl)-4-ethyl-5-methylsulfanyl-4H-[1,2,4]triazole

Guidance literature:: With sodium hydroxide; In ethanol; Ambient temperature;

Reference yield:

: 26131-22-6
1-(4-chloro-benzoyl)-4-ethyl-thiosemicarbazide

: 31409-18-4
3-(4-chloro-phenyl)-4-ethyl-5-methylsulfanyl-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 1M aq. NaHCO₃ / 24 h / Heating

2: 82 percent / aq. NaOH / ethanol / Ambient temperature

With sodium hydroxide; sodium hydrogencarbonate; In ethanol;

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 31409-18-4
3-(4-chloro-phenyl)-4-ethyl-5-methylsulfanyl-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / pyridine / 17 h / Ambient temperature

2: 68 percent / 1M aq. NaHCO₃ / 24 h / Heating

3: 82 percent / aq. NaOH / ethanol / Ambient temperature

With pyridine; sodium hydroxide; sodium hydrogencarbonate; In ethanol;