Technology Process of 2,4-Dihydroxy-3,6-dimethylbenzaldehyde
There total 9 articles about 2,4-Dihydroxy-3,6-dimethylbenzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N,N-dimethyl-formamide;
With
trichlorophosphate;
at 0 ℃;
for 0.5h;
Inert atmosphere;
2,5-dimethyl-1,3-benzenediol;
at 0 - 20 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / 0 - 18 °C / Inert atmosphere
3.1: hydrogenchloride / tetrahydrofuran; 1,4-dioxane / 20 °C
4.1: sodium cyanoborohydride; hydrogenchloride / tetrahydrofuran; water / 3 h / 20 °C
5.1: trichlorophosphate / 0.5 h / 0 °C / Inert atmosphere
5.2: 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; n-butyllithium; sodium cyanoborohydride; N-ethyl-N,N-diisopropylamine; trichlorophosphate;
In
tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / 0 - 18 °C / Inert atmosphere
2.1: hydrogenchloride / tetrahydrofuran; 1,4-dioxane / 20 °C
3.1: sodium cyanoborohydride; hydrogenchloride / tetrahydrofuran; water / 3 h / 20 °C
4.1: trichlorophosphate / 0.5 h / 0 °C / Inert atmosphere
4.2: 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; n-butyllithium; sodium cyanoborohydride; trichlorophosphate;
In
tetrahydrofuran; 1,4-dioxane; hexane; water;
