trans-1,3-Cyclobutanedicarboxylic acid 1-methyl ester

Base Information

• Chemical Name: trans-1,3-Cyclobutanedicarboxylic acid 1-methyl ester
• CAS No.: 1401103-71-6
• Molecular Formula: C₇H₁₀O₄
• Molecular Weight: 158.154
• Mol file: 1401103-71-6.mol

Synonyms:trans-1,3-Cyclobutanedicarboxylic acid 1-methyl ester;trans-3-(methoxycarbonyl)cyclobutane-1-carboxylic acid

Chemical Property of trans-1,3-Cyclobutanedicarboxylic acid 1-methyl ester

Chemical Property:

• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

trans-3-(Methoxycarbonyl)cyclobutanecarboxylicacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of trans-1,3-Cyclobutanedicarboxylic acid 1-methyl ester

There total 21 articles about trans-1,3-Cyclobutanedicarboxylic acid 1-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl 3-oxo-2-oxabicyclo<2.2.0>hept-5-ene-6-carboxylate (61752-11-2) → cis-1,3-cyclobutanedicarboxylic acid monomethyl ester (142733-61-7,116569-00-7,1401103-71-6)

Guidance literature:

With platinum on carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 16h; under 760.051 Torr;

DOI:10.1016/j.tet.2018.12.037

Reference yield: 91.0%

methanol (67-56-1) + cis-cyclobutane-1,3-dicarboxylic acid anhydride (4462-97-9) → cis-1,3-cyclobutanedicarboxylic acid monomethyl ester (142733-61-7,116569-00-7,1401103-71-6)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 10h; Ambient temperature;

Reference yield: 87.0%

cyclobutane-1,3-dicarboxylic acid dimethyl ester (90199-98-7) → cyclobutane-1,3-dicarboxylic acid monomethyl ester (1401103-71-6)

Guidance literature:

With water; sodium hydroxide; In methanol; at 20 ℃;

upstream raw materials:

methanol

cis-1,3-Cyclobutandicarbonsaeureanhydrid

cis-cyclobutane-1,3-dicarboxylic acid anhydride

7‐phenyl‐6,8‐dioxaspiro[3.5]nonane‐2,2‐dicarboxylic acid

Downstream raw materials:

C₃₂H₃₇NO₉S

3-(2-(methylthio)phenyl)-6-(3,4,5-trimethoxyphenyl)-3-azabicyclo[3.1.1]heptane-2,4-dione

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