[2-[2-(2,4-Di-tert-pentylphenoxy)hexanoylamino]-4-hydroxy-5-nitrophenoxy]acetic acid methyl ester

Base Information

Chemical Name:[2-[2-(2,4-Di-tert-pentylphenoxy)hexanoylamino]-4-hydroxy-5-nitrophenoxy]acetic acid methyl ester
CAS No.:119142-65-3
Molecular Formula:C₃₁H₄₄N₂O₈
Molecular Weight:572.699
Hs Code.:
Mol file:119142-65-3.mol

Synonyms:[2-[2-(2,4-Di-tert-pentylphenoxy)hexanoylamino]-4-hydroxy-5-nitrophenoxy]acetic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2-[2-(2,4-Di-tert-pentylphenoxy)hexanoylamino]-4-hydroxy-5-nitrophenoxy]acetic acid methyl ester

Chemical Property:

Boiling Point:678.0±55.0 °C(Predicted)
PKA:6.68±0.27(Predicted)
PSA：139.91000
Density:1.158±0.06 g/cm3(Predicted)
LogP:7.39990

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of [2-[2-(2,4-Di-tert-pentylphenoxy)hexanoylamino]-4-hydroxy-5-nitrophenoxy]acetic acid methyl ester

There total 7 articles about [2-[2-(2,4-Di-tert-pentylphenoxy)hexanoylamino]-4-hydroxy-5-nitrophenoxy]acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 67-56-1
methanol

: 2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure<4-(4-fluorphenyl-ureido)-5-hydroxy-2-methoxycarbonylmethoxyanilid>

: 119142-65-3
2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-hydroxy-2-methoxycarbonylmethoxy-4-nitranilid)

Guidance literature:: With sulfuric acid; for 4h; Heating;
DOI:10.1002/prac.19953370186

Reference yield:

: 1568-70-3
4-methoxy-2-nitrophenol

: 119142-65-3
2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-hydroxy-2-methoxycarbonylmethoxy-4-nitranilid)

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / 10percent Pd/C / dioxane

2: dioxane / 0.25 h / Heating

3: 84 percent / NaOH, Tetrabutylammoniumiodid / toluene / 0.25 h / 40 - 50 °C

4: 85 percent / 65percent aq. HNO₃, AcOH / 0.5 h / Ambient temperature

5: 85 percent / LiI, quinoline / 0.33 h / 140 - 180 °C

6: 93 percent / H₂SO₄ / 4 h / Heating

With quinoline; sodium hydroxide; sulfuric acid; hydrogen; nitric acid; tetra-(n-butyl)ammonium iodide; acetic acid; lithium iodide; palladium on activated charcoal; In 1,4-dioxane; toluene;
DOI:10.1002/prac.19953370186

Reference yield:

: 89-39-4
1,4-dimethoxy-2-nitrobenzene

: 119142-65-3
2-<2,4-Bis(1,1-dimethylpropyl)phenoxy>hexansaeure(5-hydroxy-2-methoxycarbonylmethoxy-4-nitranilid)

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / LiI, quinoline / 0.25 h / 160 - 170 °C

2: H₂ / 10percent Pd/C / dioxane

3: dioxane / 0.25 h / Heating

4: 84 percent / NaOH, Tetrabutylammoniumiodid / toluene / 0.25 h / 40 - 50 °C

5: 85 percent / 65percent aq. HNO₃, AcOH / 0.5 h / Ambient temperature

6: 85 percent / LiI, quinoline / 0.33 h / 140 - 180 °C

7: 93 percent / H₂SO₄ / 4 h / Heating

With quinoline; sodium hydroxide; sulfuric acid; hydrogen; nitric acid; tetra-(n-butyl)ammonium iodide; acetic acid; lithium iodide; palladium on activated charcoal; In 1,4-dioxane; toluene;
DOI:10.1002/prac.19953370186