Indolizine, octahydro-8-methoxy-1,2,7-tris(phenylmethoxy)-, 1S-(1.alpha.,2.beta.,7.alpha.,8.alpha.,8a.alpha.)-

Base Information

Chemical Name:Indolizine, octahydro-8-methoxy-1,2,7-tris(phenylmethoxy)-, 1S-(1.alpha.,2.beta.,7.alpha.,8.alpha.,8a.alpha.)-
CAS No.:171925-43-2
Molecular Formula:C₃₀H₃₅NO₄
Molecular Weight:473.612
Hs Code.:
Mol file:171925-43-2.mol

Synonyms:Indolizine, octahydro-8-methoxy-1,2,7-tris(phenylmethoxy)-, 1S-(1.alpha.,2.beta.,7.alpha.,8.alpha.,8a.alpha.)-

Suppliers and Price of Indolizine, octahydro-8-methoxy-1,2,7-tris(phenylmethoxy)-, 1S-(1.alpha.,2.beta.,7.alpha.,8.alpha.,8a.alpha.)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Indolizine, octahydro-8-methoxy-1,2,7-tris(phenylmethoxy)-, 1S-(1.alpha.,2.beta.,7.alpha.,8.alpha.,8a.alpha.)-

Chemical Property:

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Technology Process of Indolizine, octahydro-8-methoxy-1,2,7-tris(phenylmethoxy)-, 1S-(1.alpha.,2.beta.,7.alpha.,8.alpha.,8a.alpha.)-

There total 1 articles about Indolizine, octahydro-8-methoxy-1,2,7-tris(phenylmethoxy)-, 1S-(1.alpha.,2.beta.,7.alpha.,8.alpha.,8a.alpha.)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79831-76-8
(1S,6S,7R,8R,8aR)-2,6,7,8-tetrahydroxy-indolizidine

: 100-39-0
benzyl bromide

: 74-88-4
methyl iodide

: 171925-42-1
1,6,7-tri-O-benzyl-8-O-methylcastanospermine

: 171925-43-2
1,2,7-tri-O-benzyl-8-O-methyl-1(R),2(S)7(S),8(R),8a(R)-tetrahydroxyoctahydroindolizidine

Guidance literature:: With 1-thiopropane; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) MePh, reflux, 2 h, 2.) MePh, reflux, 3 days, 3.) DMSO, 4.) DMSO;
DOI:10.1016/0040-4020(95)00803-G

Reference yield:

: 171925-43-2
1,2,7-tri-O-benzyl-8-O-methyl-1(R),2(S)7(S),8(R),8a(R)-tetrahydroxyoctahydroindolizidine

: 171925-45-4
8-O-methyl-1(R),2(S),7(S),8(R),8a(R)-tetrahydroxyoctahydroindolizidine

Guidance literature:: With hydrogen; palladium dihydroxide; In acetic acid; for 72h; under 2068.6 Torr; Yield given;
DOI:10.1016/0040-4020(95)00803-G