tert-butyl 2-carbaMoylpiperazine-1-carboxylate

Base Information

• Chemical Name: tert-butyl 2-carbaMoylpiperazine-1-carboxylate
• CAS No.: 1246030-06-7
• Molecular Formula: C₁₀H₁₉N₃O₃
• Molecular Weight: 229.279
• Hs Code.: 2933599090
• Mol file: 1246030-06-7.mol

Synonyms:tert-butyl 2-carbaMoylpiperazine-1-carboxylate;2-Carbamoyl-piperazine-1-carboxylic acid tert-butyl ester;2-(Aminocarbonyl)-1-piperazinecarboxylic acid 1,1-dimethylethyl ester

Chemical Property of tert-butyl 2-carbaMoylpiperazine-1-carboxylate

Chemical Property:

• PSA: 84.66000
• LogP: 0.64760
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99%, ^*data from raw suppliers

tert-Butyl2-Carbamoylpiperazine-1-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl 2-carbaMoylpiperazine-1-carboxylate

There total 4 articles about tert-butyl 2-carbaMoylpiperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

piperazine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester (129799-15-1) → 2-(aminocarbonyl)-1-piperazinecarboxylic acid 1,1-dimethylethyl ester (1246030-06-7)

Guidance literature:

With ammonia; In methanol; at 60 ℃; for 72h; Inert atmosphere; Sealed tube;

Reference yield: 42.0%

methanol (67-56-1) + 1-t-Butoxycarbonylpiperazine (57260-71-6) → 2-(aminocarbonyl)-1-piperazinecarboxylic acid 1,1-dimethylethyl ester (1246030-06-7)

Guidance literature:

With ammonia; at 60 ℃; for 72h; Sealed tube;

Reference yield:

(S)-piperazine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester (796096-64-5) → (S)-tert-butyl 2-carbamoylpiperazine-1-carboxylate (1246030-06-7)

Guidance literature:

With ammonia; In methanol; at 60 ℃; for 72h; Sealed tube;

upstream raw materials:

piperazine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester

methanol

1-t-Butoxycarbonylpiperazine

(S)-piperazine-1,2-dicarboxylic acid 1-tert-butyl ester 2-methyl ester

Downstream raw materials:

2-carbamoylpiperazine-1,4-dicarboxylic acid di-tert-butyl ester

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