N-benzyl-2-(cyclohex-1-en-1-yl)ethanamine

Base Information

• Chemical Name: N-benzyl-2-(cyclohex-1-en-1-yl)ethanamine
• CAS No.: 118647-00-0
• Molecular Formula: C15H21N
• Molecular Weight: 215.338
• Mol file: 118647-00-0.mol

Synonyms:CHEMBRDG-BB 6610361;N-BENZYL-2-CYCLOHEX-1-EN-1-YLETHANAMINE;UKRORGSYN-BB BBR-013316;N-benzyl-2-cyclohex-1-en-1-ylethanamine(SALTDATA: HCl)

Chemical Property of N-benzyl-2-(cyclohex-1-en-1-yl)ethanamine

Chemical Property:

• Vapor Pressure: 0.00022mmHg at 25°C
• Boiling Point: 326.2°C at 760 mmHg
• Flash Point: 149.8°C
• Density: 0.972g/cm³

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-benzyl-2-(cyclohex-1-en-1-yl)ethanamine

There total 12 articles about N-benzyl-2-(cyclohex-1-en-1-yl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4-nitrophenyl bis(carboethoxy) benzylylide + 2-(1-cyclohexenyl)ethylamine (3399-73-3) → N-[2-(cyclohexen-1-yl)ethyl]phenylmethanamine (118647-00-0)

Guidance literature:

With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 12h; Molecular sieve;

DOI:10.1016/j.cclet.2021.06.069

Reference yield: 80.0%

2-(cyclohex-1-en-1-yl)ethyl 4-methylbenzenesulfonate (3399-72-2) + benzylamine (100-46-9) → N-[2-(cyclohexen-1-yl)ethyl]phenylmethanamine (118647-00-0)

Guidance literature:

In ethanol; for 12h; Reflux;

DOI:10.1021/jacs.8b11793

Reference yield: 72.0%

benzaldehyde (100-52-7) + 2-(1-cyclohexenyl)ethylamine (3399-73-3) → N-[2-(cyclohexen-1-yl)ethyl]phenylmethanamine (118647-00-0)

Guidance literature:

With formic acid; boron trifluoride diethyl etherate; In acetonitrile; at 85 ℃; for 1.5h; Green chemistry;

DOI:10.1039/d1gc01468d

upstream raw materials:

N-(2-(cyclohex-1-en-1-yl)ethyl)-1-phenylmethanimine

benzaldehyde

2-(1-cyclohexenyl)ethylamine

1-ethenylcyclohexene

Downstream raw materials:

benzyl-[2-(1,2-dibromo-cyclohexyl)-ethyl]-amine

N-benzyl-N-chloro-2-cyclohex-1-enylethylamine