2,4-Bis([1,1'-biphenyl]-4-yl)-6-chloro-1,3,5-triazine

Base Information

• Chemical Name: 2,4-Bis([1,1'-biphenyl]-4-yl)-6-chloro-1,3,5-triazine
• CAS No.: 182918-13-4
• Molecular Formula: C27H18ClN3
• Molecular Weight: 419.90492
• Mol file: 182918-13-4.mol

Synonyms:2,4-Bis([1,1'-biphenyl]-4-yl)-6-chloro-1,3,5-triazine;2,4-di(biphenyl-4-yl)-6-chloro-1,3,5-triazine;2-chloro-4,6-di(biphenyl-4-yl)-1,3,5-triazine;1,3,5-Triazine, 2,4-bis([1,1'-biphenyl]-4-yl)-6-chloro-;2,4-Bis(4-biphenylyl)-6-chloro-1,3,5-triazine;2,4-Di([1,1'-biphenyl]-4-yl)-6-chloro-1,3,5-triazine;2-chloro-4,6-bis(4-biphenylyl)-1,3,5-triazine;2,4-Bis-biphenyl-4-yl-6-chloro-[1,3,5]triazine

Chemical Property of 2,4-Bis([1,1'-biphenyl]-4-yl)-6-chloro-1,3,5-triazine

Chemical Property:

• Melting Point: 215.0 to 219.0 °C
• Boiling Point: 649.6±58.0 °C(Predicted)
• PKA: 0.28±0.10(Predicted)
• PSA: 38.67000
• Density: 1.227±0.06 g/cm3(Predicted)
• LogP: 7.19300
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

≥99% ^*data from raw suppliers

2,4-Bis(4-biphenylyl)-6-chloro-1,3,5-triazine >98.0%(HPLC)(N) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 2,4-Bis([1,1'-biphenyl]-4-yl)-6-chloro-1,3,5-triazine is used in photoelectric materials; semiconductor building blocks; synthetic material intermediates, etc.

Technology Process of 2,4-Bis([1,1'-biphenyl]-4-yl)-6-chloro-1,3,5-triazine

There total 10 articles about 2,4-Bis([1,1'-biphenyl]-4-yl)-6-chloro-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.6%

2,4-bis([1,1'-biphenyl]-4-yl)-6-hydroxy-1,3,5-triazine → 2,4‐bis({[1,1'‐biphenyl]‐4‐yl})‐6‐chloro‐1,3,5‐triazine (182918-13-4)

Guidance literature:

With thionyl chloride; In N,N-dimethyl-formamide; 1,2-dichloro-benzene; at 78 ℃; for 5h;

Reference yield: 76.2%

4-biphenyllithium (1201-71-4) + 2‐{[1,1'‐biphenyl]‐4‐yl}‐4,6‐dichloro‐1,3,5‐triazine (10202-45-6) → 2,4‐bis({[1,1'‐biphenyl]‐4‐yl})‐6‐chloro‐1,3,5‐triazine (182918-13-4)

Guidance literature:

In tetrahydrofuran; at -20 - 0 ℃; for 2h; Temperature;

Reference yield: 75.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + 4-bromo-1,1'-biphenyl (92-66-0) → 2,4‐bis({[1,1'‐biphenyl]‐4‐yl})‐6‐chloro‐1,3,5‐triazine (182918-13-4)

Guidance literature:

4-bromo-1,1'-biphenyl; With n-butyllithium; In tetrahydrofuran; at -70 ℃; for 1h; Inert atmosphere;

1,3,5-trichloro-2,4,6-triazine; In tetrahydrofuran; for 2h;

upstream raw materials:

1,3,5-trichloro-2,4,6-triazine

4-bromo-1,1'-biphenyl

4-biphenylylmagnesium bromide

biphenyl

Downstream raw materials:

2,4-bis(biphenyl-4-yl)-6-(3,5-dibromophenyl)-1,3,5-triazine