Phenyl[5-(dimethylamino)-1-naphtylsulfonyl] ether

Base Information

• Chemical Name: Phenyl[5-(dimethylamino)-1-naphtylsulfonyl] ether
• CAS No.: 55837-12-2
• Molecular Formula: C18H17NO3S
• Molecular Weight: 327.404
• Mol file: 55837-12-2.mol

Synonyms:5-(Dimethylamino)-1-naphthalenesulfonic acid phenyl ester;Phenyl[5-(dimethylamino)-1-naphtylsulfonyl] ether

Chemical Property of Phenyl[5-(dimethylamino)-1-naphtylsulfonyl] ether

Chemical Property:

• PSA: 54.99000
• LogP: 4.75430

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phenyl[5-(dimethylamino)-1-naphtylsulfonyl] ether

There total 1 articles about Phenyl[5-(dimethylamino)-1-naphtylsulfonyl] ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5-(dimethylamino)naphth-1-ylsulfonyl chloride (605-65-2) + phenol (108-95-2,27073-41-2) → 5-dimethylamino-naphthalene-1-sulfonic acid phenyl ester (55837-12-2)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane;

DOI:10.1021/jo1007338

Reference yield: 59.0%

O-tosyl-N-trichloroethoxycarbonylhydroxylamine (931109-52-3) + 5-dimethylamino-naphthalene-1-sulfonic acid phenyl ester (55837-12-2) → phenyl 5-(methyl((((2,2,2-trichloroethoxy)carbonyl)amino)methyl)amino)naphthalene-1-sulfonate

Guidance literature:

With C₁₄H₃₃O₂Rh₂; potassium carbonate; In toluene; at 20 ℃; for 12h; chemoselective reaction;

DOI:10.1055/a-1334-6450

upstream raw materials:

5-(dimethylamino)naphth-1-ylsulfonyl chloride

phenol

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