1,3-DiMethyl 2-[4-(Methoxycarbonyl)-2-nitrophenyl]propanedioate

Base Information

Chemical Name:1,3-DiMethyl 2-[4-(Methoxycarbonyl)-2-nitrophenyl]propanedioate
CAS No.:1160293-27-5
Molecular Formula:C13H13NO8
Molecular Weight:311.248
Hs Code.:2918990090
Mol file:1160293-27-5.mol

Synonyms:1,3-DiMethyl 2-[4-(Methoxycarbonyl)-2-nitrophenyl]propanedioate;dimethyl 2-(4-methoxycarbonyl-2-nitrophenyl)propanedioate;methyl 4-(di(methoxycarbonyl)methyl)-3-nitrobenzoate;2-[4-(Methoxycarbonyl)-2-nitrophenyl]propanedioic acid 1,3-dimethyl ester;[4-(methoxycarbonyl)-2-nitrophenyl]-propanedioic acid dimethyl ester;dimethyl 2-(4-(methoxycarbonyl)-2-nitrophenyl)malonate

Suppliers and Price of 1,3-DiMethyl 2-[4-(Methoxycarbonyl)-2-nitrophenyl]propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1,3-Dimethyl2-[4-(methoxycarbonyl)-2-nitrophenyl]propanedioate
250mg
$ 50.00

Crysdot
1,3-Dimethyl2-[4-(methoxycarbonyl)-2-nitrophenyl]propanedioate 95+%
25g
$ 456.00

Alichem
1,3-Dimethyl2-[4-(methoxycarbonyl)-2-nitrophenyl]propanedioate
25g
$ 474.24

AK Scientific
1,3-Dimethyl2-[4-(methoxycarbonyl)-2-nitrophenyl]propanedioate
25g
$ 641.00

AK Scientific
1,3-Dimethyl2-[4-(methoxycarbonyl)-2-nitrophenyl]propanedioate
25g
$ 480.00

AK Scientific
1,3-Dimethyl2-[4-(methoxycarbonyl)-2-nitrophenyl]propanedioate
10g
$ 280.00

AK Scientific
1,3-Dimethyl2-[4-(methoxycarbonyl)-2-nitrophenyl]propanedioate
5g
$ 241.00

Total 26 raw suppliers

Chemical Property of 1,3-DiMethyl 2-[4-(Methoxycarbonyl)-2-nitrophenyl]propanedioate

Chemical Property:

Boiling Point:433.1±40.0 °C(Predicted)
PKA:9.81±0.46(Predicted)
PSA：124.72000
Density:1.357±0.06 g/cm3(Predicted)
LogP:1.33420
Storage Temp.:Refrigerator, under inert atmosphere
Solubility.:Chloroform (Slightly), Ethyl Acetate (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

1,3-Dimethyl2-[4-(methoxycarbonyl)-2-nitrophenyl]propanedioate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-DiMethyl 2-[4-(Methoxycarbonyl)-2-nitrophenyl]propanedioate

There total 2 articles about 1,3-DiMethyl 2-[4-(Methoxycarbonyl)-2-nitrophenyl]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.4%

: 14719-83-6
methyl 3-nitro-4-chlorobenzoate

: 108-59-8
malonic acid dimethyl ester

: 1160293-27-5
[4-(methoxycarbonyl)-2-nitrophenyl]malonic acid dimethyl ester

Guidance literature:: With sodium tert-pentoxide; In 1-methyl-pyrrolidin-2-one; at 75 ℃; for 1.5h;

Reference yield:

: 96-99-1
4-chloro-3-nitrobenzoate

: 1160293-27-5
[4-(methoxycarbonyl)-2-nitrophenyl]malonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 3 h / 70 °C

2: sodium tert-pentoxide / 1-methyl-pyrrolidin-2-one / 1.5 h / 75 °C

With thionyl chloride; sodium tert-pentoxide; In 1-methyl-pyrrolidin-2-one;