Technology Process of 2'-PHENYL-[2,5']BIOXAZOLYL
There total 6 articles about 2'-PHENYL-[2,5']BIOXAZOLYL which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
nickel(IV) oxide;
In
benzene;
for 2h;
Heating;
DOI:10.1007/BF00575250
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 85 percent / POCl3 / 1) 0-5 deg C,10min. 2) 7 h, 95 deg C
2: 77 percent / Sulfuric acid, CrO3 / acetone; H2O / 1 h / 20 °C
3: 97 percent / conc. Sulfuric acid / 6 h / Heating
4: 3 h / 150 °C
5: 1)SOCl2 2)KOH / 1) 1h, 60 deg C 2)benzene, H2O, reflux 2.5 h
6: 39 percent / Nickel peroxide / benzene / 2 h / Heating
With
chromium(VI) oxide; nickel(IV) oxide; potassium hydroxide; thionyl chloride; sulfuric acid; trichlorophosphate;
In
water; acetone; benzene;
DOI:10.1007/BF00575250
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 77 percent / Sulfuric acid, CrO3 / acetone; H2O / 1 h / 20 °C
2: 97 percent / conc. Sulfuric acid / 6 h / Heating
3: 3 h / 150 °C
4: 1)SOCl2 2)KOH / 1) 1h, 60 deg C 2)benzene, H2O, reflux 2.5 h
5: 39 percent / Nickel peroxide / benzene / 2 h / Heating
With
chromium(VI) oxide; nickel(IV) oxide; potassium hydroxide; thionyl chloride; sulfuric acid;
In
water; acetone; benzene;
DOI:10.1007/BF00575250
