6-Chloro-5-nitropicolinic acid

Base Information

Chemical Name:6-Chloro-5-nitropicolinic acid
CAS No.:353277-27-7
Molecular Formula:C6H3ClN2O4
Molecular Weight:202.554
Hs Code.:2933399090
DSSTox Substance ID:DTXSID10361038
Wikidata:Q82143131
Mol file:353277-27-7.mol

Synonyms:6-Chloro-5-nitropicolinic acid;353277-27-7;6-chloro-5-nitropyridine-2-carboxylic acid;MFCD01927937;6-Chloro-5-nitropicolinicacid;SCHEMBL805289;AMY2011;DTXSID10361038;AKOS016012810;CS-W006408;DS-5471;SY109252;FT-0701619;EN300-110367;A874633;6-Chloro-5-nitropyridine-2-carboxylic acid

Suppliers and Price of 6-Chloro-5-nitropicolinic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
6-Chloro-5-nitropicolinicAcid
10mg
$ 65.00

Crysdot
6-Chloro-5-nitropicolinicacid 98%
5g
$ 847.00

Crysdot
6-Chloro-5-nitropicolinicacid 98%
1g
$ 282.00

Crysdot
6-Chloro-5-nitropicolinicacid 98%
10g
$ 1337.00

Chemenu
6-chloro-5-nitropicolinicacid 98%
10g
$ 1262.00

Chemenu
6-chloro-5-nitropicolinicacid 98%
1g
$ 267.00

Chemenu
6-chloro-5-nitropicolinicacid 98%
5g
$ 800.00

Chemcia Scientific
6-Chloro-5-nitro-pyridine-2-carboxylicacid ＞97%
5 G
$ 785.00

American Custom Chemicals Corporation
6-CHLORO-5-NITROPYRIDINE-2-CARBOXYLIC ACID 95.00%
5MG
$ 505.58

Ambeed
6-Chloro-5-nitropicolinicacid 98%
10g
$ 1427.00

Total 18 raw suppliers

Chemical Property of 6-Chloro-5-nitropicolinic acid

Chemical Property:

Boiling Point:413.6±45.0 °C(Predicted)
PKA:2.34±0.13(Predicted)
PSA：96.01000
Density:1.702±0.06 g/cm3(Predicted)
LogP:1.86460
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:201.9781343
Heavy Atom Count:13
Complexity:229

Purity/Quality:

97% ^*data from raw suppliers

6-Chloro-5-nitropicolinicAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=NC(=C1[N+](=O)[O-])Cl)C(=O)O

Technology Process of 6-Chloro-5-nitropicolinic acid

There total 4 articles about 6-Chloro-5-nitropicolinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 56057-19-3
2-chloro-6-methyl-3-nitropyridine

: 353277-27-7
6-chloro-5-nitropyridine-2-carboxylic acid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; at 15 - 50 ℃; for 20h;

Reference yield:

: 21901-29-1
6-amino-5-nitro-2-picoline

: 353277-27-7
6-chloro-5-nitropyridine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: water; sodium nitrite; sulfuric acid / 16 h / 0 °C

2: trichlorophosphate / 4 h / Reflux

3: sodium dichromate; sulfuric acid / 40 h / 30 °C

With sodium dichromate; sulfuric acid; water; sodium nitrite; trichlorophosphate;

Reference yield:

: 39745-39-6
6-methyl-3-nitrohydropyridin-2-one

: 353277-27-7
6-chloro-5-nitropyridine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 4 h / Reflux

2: sodium dichromate; sulfuric acid / 40 h / 30 °C

With sodium dichromate; sulfuric acid; trichlorophosphate;