4-Oxazolecarbothioamide,5-ethoxy-N,2-dimethyl-(9CI)

Base Information

Chemical Name:4-Oxazolecarbothioamide,5-ethoxy-N,2-dimethyl-(9CI)
CAS No.:128269-81-8
Molecular Formula:C₈H₁₂N₂O₂S
Molecular Weight:200.261
Hs Code.:
Mol file:128269-81-8.mol

Synonyms:4-Oxazolecarbothioamide,5-ethoxy-N,2-dimethyl-(9CI);5-ethoxy-N,2-dimethyl-4-oxazolecarbothioamide

Suppliers and Price of 4-Oxazolecarbothioamide,5-ethoxy-N,2-dimethyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-ETHOXY-N-2-DIMETHYLOXAZOLE-4-CARBOTHIOAMIDE 95.00%
5MG
$ 495.91

Total 3 raw suppliers

Chemical Property of 4-Oxazolecarbothioamide,5-ethoxy-N,2-dimethyl-(9CI)

Chemical Property:

PSA：79.38000
LogP:1.66750

Purity/Quality:

98%min ^*data from raw suppliers

5-ETHOXY-N-2-DIMETHYLOXAZOLE-4-CARBOTHIOAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Oxazolecarbothioamide,5-ethoxy-N,2-dimethyl-(9CI)

There total 5 articles about 4-Oxazolecarbothioamide,5-ethoxy-N,2-dimethyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 128242-88-6
2-methyl-4-<(N-methylamino)carbonyl>-5-ethoxyoxazole

: 128242-99-9
2-methyl-4-(ethoxycarbonyl)-5-(N-methylamino)thiazole

: 128269-81-8
2-methyl-4-<(N-methylamino)thiocarbonyl>-5-ethoxyoxazole

Guidance literature:: With Lawessons reagent; In tetrahydrofuran;
DOI:10.1021/jo00301a056

Reference yield: 38.0%

: 3356-83-0
2-methyl-4-(methylaminocarbonyl)-5-ethoxyoxazole

: 128269-81-8
2-methyl-4-<(N-methylamino)thiocarbonyl>-5-ethoxyoxazole

: 31785-05-4
5-amino-2-methyl-1,3-thiazole-4-carboxylic acid ethyl ester

Guidance literature:: With Lawessons reagent; In tetrahydrofuran; for 2h; Heating;
DOI:10.1021/jo00301a056

Reference yield:

: 3357-56-0
2-methyl-5-ethoxyoxazole-4-carboxylic acid

: 128269-81-8
2-methyl-4-<(N-methylamino)thiocarbonyl>-5-ethoxyoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, DMF / CH₂Cl₂ / 2 h / Ambient temperature

2: 82 percent / H₂O

3: 38 percent / 2,4-bis(methoxyphenyl)-1,3-dithia-2,4-diphosphetane 2,4-disulfide (Lawesson's reagent) / tetrahydrofuran

With Lawessons reagent; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo00301a056