ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate

Base Information Edit

Chemical Name:ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate
CAS No.:1448869-67-7
Molecular Formula:C9H13BrN2O2
Molecular Weight:261.118
Hs Code.:
Mol file:1448869-67-7.mol

Synonyms:ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate;2-bromo-1-isopropyl-1H-imidazole-4-carboxylic acid ethyl ester

Suppliers and Price of ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
Ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate 95%+
250mg
$ 517.00

Chemenu
Ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate 95%+
100mg
$ 334.00

Chemenu
Ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate 95%+
1g
$ 1313.00

A1 Biochem Labs
Ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate 95%
2.5 g
$ 1200.00

Total 5 raw suppliers

Chemical Property of ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate Edit

Chemical Property:

Boiling Point:336.1±34.0 °C(Predicted)
PKA:0.61±0.60(Predicted)
PSA：44.12000
Density:1.46±0.1 g/cm3(Predicted)
LogP:2.40320

Purity/Quality:

NLT 98% ^*data from raw suppliers

Ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate

There total 9 articles about ethyl2-bromo-1-isopropyl-1H-imidazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.85%

: 1260793-84-7
1-isopropyl-1H-imidazole-4-carboxylic acid ethyl ester

: 1448869-67-7
2-bromo-1-isopropyl-1H-imidazole-4-carboxylic acid ethyl ester

Guidance literature:: With potassium phosphate; N-Bromosuccinimide; In tetrahydrofuran; at 25 ℃; for 12h; Large scale;

Reference yield:

: 1260793-84-7
1-isopropyl-1H-imidazole-4-carboxylic acid ethyl ester

: 1448869-67-7
2-bromo-1-isopropyl-1H-imidazole-4-carboxylic acid ethyl ester

: ethyl-5-bromo-1-isopropyl-1H-imidazole-4-carboxylate

Guidance literature:: With N-Bromosuccinimide; In tetrahydrofuran; at 25 ℃;
DOI:10.1016/j.bmcl.2018.08.027

Reference yield:

: 2999-46-4
Ethyl isocyanoacetate

: 1448869-67-7
2-bromo-1-isopropyl-1H-imidazole-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 30 h / 20 °C / Inert atmosphere

2: butan-1-ol / 15 h / 130 °C / Inert atmosphere

3: N-Bromosuccinimide / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; In tetrahydrofuran; ethanol; butan-1-ol;