Pyrrolo[3,4-c]pyrrole, octahydro-2-Methyl-5-(6-phenyl-3-pyridazinyl)-

Base Information

• Chemical Name: Pyrrolo[3,4-c]pyrrole, octahydro-2-Methyl-5-(6-phenyl-3-pyridazinyl)-
• CAS No.: 848591-89-9
• Molecular Formula: C₁₇H₂₀N₄
• Molecular Weight: 280.373
• Hs Code.: 2933990090
• Mol file: 848591-89-9.mol

Synonyms:Pyrrolo[3,4-c]pyrrole, octahydro-2-Methyl-5-(6-phenyl-3-pyridazinyl)-;2-Methyl-5-(6-phenylpyridazin-3-yl)octahydropyrrolo[3,4-c]pyrrole

Chemical Property of Pyrrolo[3,4-c]pyrrole, octahydro-2-Methyl-5-(6-phenyl-3-pyridazinyl)-

Chemical Property:

• PSA: 32.26000
• LogP: 2.14430
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-Methyl-5-(6-phenylpyridazin-3-yl)octahydropyrrolo[3,4-c]pyrrole 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Pyrrolo[3,4-c]pyrrole, octahydro-2-Methyl-5-(6-phenyl-3-pyridazinyl)-

There total 5 articles about Pyrrolo[3,4-c]pyrrole, octahydro-2-Methyl-5-(6-phenyl-3-pyridazinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2-(6-phenyl-pyridazin-3-yl)-octahydro-pyrrolo[3,4-c]pyrrole (848591-85-5) + formaldehyd (50-00-0,30525-89-4,61233-19-0) → octahydro-2-methyl-5-(6-phenyl-3-pyridazinyl)-pyrrolo[3,4-c]pyrrole (848591-89-9)

Guidance literature:

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 16h;

Reference yield: 76.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + formic acid (64-18-6) + tert-butyl cis-5-(6-phenylpyridazine-3-yl)-hexahydro-pyrrolo[3,4-c]-pyrrole-2(1H)-carboxylate (1173179-74-2) → A-582941 (1173179-34-4,848591-89-9)

Guidance literature:

at 100 ℃; for 1h;

Reference yield: 53.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + tert-butyl cis-5-(6-phenylpyridazine-3-yl)-hexahydro-pyrrolo[3,4-c]-pyrrole-2(1H)-carboxylate (1173179-74-2) → A-582941 (1173179-34-4,848591-89-9)

Guidance literature:

With formic acid; In water; at 100 ℃; for 1h;

DOI:10.1021/jm900249k

upstream raw materials:

2-(6-phenyl-pyridazin-3-yl)-octahydro-pyrrolo[3,4-c]pyrrole

formaldehyd

tert-butyl cis-5-(6-phenylpyridazine-3-yl)-hexahydro-pyrrolo[3,4-c]-pyrrole-2(1H)-carboxylate

3-chloro-6-phenylpyradazine

Downstream raw materials:

2-methyl-5-(6-phenylpyridazin-3-yl)octahydropyrrolo[3,4-c]pyrrole dihydrochloride

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