5,11,17,23-tetracyanomethyl-25,27-bis(benzoyloxy)-26,28-dihydroxycalix<4>arene

Base Information

Chemical Name:5,11,17,23-tetracyanomethyl-25,27-bis(benzoyloxy)-26,28-dihydroxycalix<4>arene
CAS No.:161316-89-8
Molecular Formula:C₅₀H₃₆N₄O₆
Molecular Weight:788.859
Hs Code.:

Synonyms:5,11,17,23-tetracyanomethyl-25,27-bis(benzoyloxy)-26,28-dihydroxycalix<4>arene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,11,17,23-tetracyanomethyl-25,27-bis(benzoyloxy)-26,28-dihydroxycalix<4>arene

Chemical Property:

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Technology Process of 5,11,17,23-tetracyanomethyl-25,27-bis(benzoyloxy)-26,28-dihydroxycalix<4>arene

There total 1 articles about 5,11,17,23-tetracyanomethyl-25,27-bis(benzoyloxy)-26,28-dihydroxycalix<4>arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 98-88-4
benzoyl chloride

: 157749-24-1,479092-35-8,115421-59-5
p-cyanomethylcalix[4]arene

: 161316-89-8
5,11,17,23-tetracyanomethyl-25,27-bis(benzoyloxy)-26,28-dihydroxycalix<4>arene

Guidance literature:: With aluminium trichloride; In dichloromethane; N,N-dimethyl-formamide; in ice bath, 20 min and room t.;
DOI:10.1055/s-1994-25581

Reference yield:

: 79-03-8
propionyl chloride

: 161316-89-8
5,11,17,23-tetracyanomethyl-25,27-bis(benzoyloxy)-26,28-dihydroxycalix<4>arene

: C₅₆H₄₄N₄O₈

Guidance literature:: With 1-methyl-1H-imidazole; Yield given. Multistep reaction; 1.) MeCN, 5-10 min and 20 min, in ice bath, 2.) MeCN, in ice bath and room t.;
DOI:10.1055/s-1994-25581

Reference yield:

: 618-46-2
m-Chlorobenzoyl chloride

: 161316-89-8
5,11,17,23-tetracyanomethyl-25,27-bis(benzoyloxy)-26,28-dihydroxycalix<4>arene

: C₆₄H₄₂Cl₂N₄O₈

Guidance literature:: With 1-methyl-1H-imidazole; Yield given. Multistep reaction; 1.) MeCN, 5-10 min and 20 min, in ice bath, 2.) MeCN, in ice bath and room t.;
DOI:10.1055/s-1994-25581