4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester 1-(2-phenylsulfanyl-ethyl) ester

Base Information

Chemical Name:4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester 1-(2-phenylsulfanyl-ethyl) ester
CAS No.:142549-48-2
Molecular Formula:C₂₅H₂₄N₂O₈S
Molecular Weight:512.54
Hs Code.:

Synonyms:4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester 1-(2-phenylsulfanyl-ethyl) ester

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Chemical Property of 4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester 1-(2-phenylsulfanyl-ethyl) ester

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Technology Process of 4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester 1-(2-phenylsulfanyl-ethyl) ester

There total 2 articles about 4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester 1-(2-phenylsulfanyl-ethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.4%

: 108-98-5
thiophenol

: 142549-47-1
4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 1-(2-chloro-ethyl) ester 3-methyl ester

: 142549-48-2
4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester 1-(2-phenylsulfanyl-ethyl) ester

Guidance literature:: With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; for 3h;
DOI:10.1248/cpb.40.899

Reference yield:

: 142549-46-0
4-Hydroxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 1-(2-chloro-ethyl) ester 3-methyl ester

: 142549-48-2
4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester 1-(2-phenylsulfanyl-ethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / K₂CO₃ / dimethylformamide / 19 h / Ambient temperature

2: 98.4 percent / NaI, K₂CO₃ / dimethylformamide / 3 h

With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.40.899