4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester

Base Information

Chemical Name:4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester
CAS No.:142549-51-7
Molecular Formula:C₁₇H₁₆N₂O₈
Molecular Weight:376.323
Hs Code.:

Synonyms:4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester

Suppliers and Price of 4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester

There total 4 articles about 4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.7%

: 142549-49-3
4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 1-(2-benzenesulfonyl-ethyl) ester 3-methyl ester

: 142549-51-7
4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; for 0.5h; Ambient temperature;
DOI:10.1248/cpb.40.899

Reference yield:

: 142549-46-0
4-Hydroxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 1-(2-chloro-ethyl) ester 3-methyl ester

: 142549-51-7
4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / K₂CO₃ / dimethylformamide / 19 h / Ambient temperature

2: 98.4 percent / NaI, K₂CO₃ / dimethylformamide / 3 h

3: 63.1 percent / m-chloroperbenzoic acid / CHCl₃ / 1 h

4: 83.7 percent / 1 N aq. NaOH / methanol; tetrahydrofuran / 0.5 h / Ambient temperature

With sodium hydroxide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.40.899

Reference yield:

: 142549-47-1
4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 1-(2-chloro-ethyl) ester 3-methyl ester

: 142549-51-7
4-Methoxymethoxy-6-methyl-2-(3-nitro-pyridin-2-yl)-isophthalic acid 3-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98.4 percent / NaI, K₂CO₃ / dimethylformamide / 3 h

2: 63.1 percent / m-chloroperbenzoic acid / CHCl₃ / 1 h

3: 83.7 percent / 1 N aq. NaOH / methanol; tetrahydrofuran / 0.5 h / Ambient temperature

With sodium hydroxide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.40.899