2,2-bis[3-(3-acetylmercaptopropyl)-4-(3-acetylmercaptopropoxy)-phenyl]propane

Base Information

Chemical Name:2,2-bis[3-(3-acetylmercaptopropyl)-4-(3-acetylmercaptopropoxy)-phenyl]propane
CAS No.:1636900-12-3
Molecular Formula:C₃₅H₄₈O₆S₄
Molecular Weight:693.027
Hs Code.:

Synonyms:2,2-bis[3-(3-acetylmercaptopropyl)-4-(3-acetylmercaptopropoxy)-phenyl]propane

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Chemical Property of 2,2-bis[3-(3-acetylmercaptopropyl)-4-(3-acetylmercaptopropoxy)-phenyl]propane

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Technology Process of 2,2-bis[3-(3-acetylmercaptopropyl)-4-(3-acetylmercaptopropoxy)-phenyl]propane

There total 4 articles about 2,2-bis[3-(3-acetylmercaptopropyl)-4-(3-acetylmercaptopropoxy)-phenyl]propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 26306-34-3
4,4’-(dimethylmethylene)bis[2-(2-propenyl)phenyl]diallyl ether

: 507-09-5
tiolacetic acid

: 1636900-12-3
2,2-bis[3-(3-acetylmercaptopropyl)-4-(3-acetylmercaptopropoxy)-phenyl]propane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In tetrahydrofuran; at 20 - 65 ℃; for 16.5h; Inert atmosphere;
DOI:10.3762/bjoc.10.180

Reference yield:

: 1745-89-7
2,2-bis(3-allyl-4-hydroxyphenyl)propane

: 1636900-12-3
2,2-bis[3-(3-acetylmercaptopropyl)-4-(3-acetylmercaptopropoxy)-phenyl]propane

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 1 h / Inert atmosphere; Reflux

1.2: Reflux; Inert atmosphere

2.1: 2,2'-azobis(isobutyronitrile) / tetrahydrofuran / 16.5 h / 20 - 65 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); potassium carbonate; In tetrahydrofuran; acetone;
DOI:10.3762/bjoc.10.180

Reference yield:

: 3739-67-1
bisphenol A diallyl ether

: 1636900-12-3
2,2-bis[3-(3-acetylmercaptopropyl)-4-(3-acetylmercaptopropoxy)-phenyl]propane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4 h / 220 °C / Inert atmosphere

2.1: potassium carbonate / acetone / 1 h / Inert atmosphere; Reflux

2.2: Reflux; Inert atmosphere

3.1: 2,2'-azobis(isobutyronitrile) / tetrahydrofuran / 16.5 h / 20 - 65 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); potassium carbonate; In tetrahydrofuran; acetone; 1.1: |Claisen Rearrangement;
DOI:10.3762/bjoc.10.180