Hexahydro-1-(2-pyridyl)-2H-azepin-2-one

Base Information

Chemical Name:Hexahydro-1-(2-pyridyl)-2H-azepin-2-one
CAS No.:51263-32-2
Molecular Formula:C11H14N2O
Molecular Weight:190.2417
Hs Code.:2933990090
Mol file:51263-32-2.mol

Synonyms:1-pyridin-2-yl-azepan-2-one;Hexahydro-1-(2-pyridyl)-2H-azepin-2-one;Azepin-2-one der.;2H-Azepin-2-one,hexahydro-1-(2-pyridyl);2H-Azepin-2-one,hexahydro-1-(2-pyridinyl);N-2-pyridylcaprolactam;

Suppliers and Price of Hexahydro-1-(2-pyridyl)-2H-azepin-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-(pyridin-2-yl)azepan-2-one
500mg
$ 65.00

Sigma-Aldrich
HEXAHYDRO-1-(2-PYRIDYL)-2H-AZEPIN-2-ONE Aldrich
1g
$ 57.00

American Custom Chemicals Corporation
1-(PYRIDIN-2-YL)AZEPAN-2-ONE 95.00%
10G
$ 1382.48

American Custom Chemicals Corporation
1-(PYRIDIN-2-YL)AZEPAN-2-ONE 95.00%
5G
$ 955.42

American Custom Chemicals Corporation
1-(PYRIDIN-2-YL)AZEPAN-2-ONE 95.00%
1G
$ 646.25

Total 5 raw suppliers

Chemical Property of Hexahydro-1-(2-pyridyl)-2H-azepin-2-one

Chemical Property:

Vapor Pressure:6.97E-07mmHg at 25°C
Boiling Point:408.5°Cat760mmHg
Flash Point:200.8°C
PSA：33.20000
Density:1.124g/cm³
LogP:2.05360

Purity/Quality:

99% ^*data from raw suppliers

1-(pyridin-2-yl)azepan-2-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Hexahydro-1-(2-pyridyl)-2H-azepin-2-one

There total 3 articles about Hexahydro-1-(2-pyridyl)-2H-azepin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 105-60-2,9012-16-2
caprolactam

: 57785-86-1
pyridin-2-yl tosylate

: 51263-32-2
N-2-pyridylcaprolactam

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; potassium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,4-dioxane; at 100 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.200903235

Reference yield: 57.0%

: 109-09-1
2-chloropyridine

: 105-60-2,9012-16-2
caprolactam

: 51263-32-2
N-2-pyridylcaprolactam

Guidance literature:: With copper(I) oxide; potassium phosphate; N¹,N²-bis(thiophen-2-ylmethyl)oxalamide; In tert-butyl alcohol; at 130 ℃; for 24h; Schlenk technique;
DOI:10.1021/acs.orglett.7b02326