(R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide

Base Information

Chemical Name:(R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide
CAS No.:1539220-76-2
Molecular Formula:C₄₁H₄₃NO₃
Molecular Weight:597.797
Hs Code.:

Synonyms:(R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide

Suppliers and Price of (R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of (R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of (R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide

There total 4 articles about (R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1539220-42-2
(R,S)-3-(2-hydroxy-5-(hydroxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide

: 1539220-76-2
(R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; sodium carbonate; In water; toluene; at 50 - 55 ℃; under 750.075 Torr; Inert atmosphere;

Reference yield:

: 1539220-70-6
3-(2-hydroxy-5-(hydroxymethyl)phenyl)-N,N-diisopropyl-3-phenylacrylamide

: 1539220-76-2
(R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 5%-palladium/activated carbon; hydrogen; sodium carbonate / 2-methyltetrahydrofuran; ethanol / 50 °C / 750.08 Torr / Inert atmosphere

2: 5%-palladium/activated carbon; hydrogen; sodium carbonate / water; toluene / 50 - 55 °C / 750.08 Torr / Inert atmosphere

With 5%-palladium/activated carbon; hydrogen; sodium carbonate; In 2-methyltetrahydrofuran; ethanol; water; toluene;

Reference yield:

: 29922-56-3
2-bromo-4-(hydroxymethyl)phenol

: 1539220-76-2
(R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-Methyldicyclohexylamine; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 2-methyltetrahydrofuran / 70 - 86 °C

2: 5%-palladium/activated carbon; hydrogen; sodium carbonate / 2-methyltetrahydrofuran; ethanol / 50 °C / 750.08 Torr / Inert atmosphere

3: 5%-palladium/activated carbon; hydrogen; sodium carbonate / water; toluene / 50 - 55 °C / 750.08 Torr / Inert atmosphere

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; N-Methyldicyclohexylamine; 5%-palladium/activated carbon; hydrogen; sodium carbonate; In 2-methyltetrahydrofuran; ethanol; water; toluene;