4-[1-(5-dimethylamino-naphthalene-1-sulfonyloxy)-2,2,2-trifluoro-ethyl]-phenyl acetate

Base Information

Chemical Name:4-[1-(5-dimethylamino-naphthalene-1-sulfonyloxy)-2,2,2-trifluoro-ethyl]-phenyl acetate
CAS No.:1279691-46-1
Molecular Formula:C₂₂H₂₀F₃NO₅S
Molecular Weight:467.466
Hs Code.:

Synonyms:4-[1-(5-dimethylamino-naphthalene-1-sulfonyloxy)-2,2,2-trifluoro-ethyl]-phenyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[1-(5-dimethylamino-naphthalene-1-sulfonyloxy)-2,2,2-trifluoro-ethyl]-phenyl acetate

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Technology Process of 4-[1-(5-dimethylamino-naphthalene-1-sulfonyloxy)-2,2,2-trifluoro-ethyl]-phenyl acetate

There total 2 articles about 4-[1-(5-dimethylamino-naphthalene-1-sulfonyloxy)-2,2,2-trifluoro-ethyl]-phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1279691-41-6
acetic acid 4-(2,2,2-trifluoro-1-hydroxyethyl)phenyl ester

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 1279691-46-1
4-[1-(5-dimethylamino-naphthalene-1-sulfonyloxy)-2,2,2-trifluoro-ethyl]-phenyl acetate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane;
DOI:10.1039/c0cc04796a

Reference yield:

: 878-00-2
4-formylphenyl acetate

: 1279691-46-1
4-[1-(5-dimethylamino-naphthalene-1-sulfonyloxy)-2,2,2-trifluoro-ethyl]-phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with ice

2: 1,4-diaza-bicyclo[2.2.2]octane / dichloromethane

With 1,4-diaza-bicyclo[2.2.2]octane; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c0cc04796a