(2S)-2-hydroxy-N-methoxy-N-methyl-3-phenylpropanamide

Base Information

Chemical Name:(2S)-2-hydroxy-N-methoxy-N-methyl-3-phenylpropanamide
CAS No.:188295-04-7
Molecular Formula:C₁₁H₁₅NO₃
Molecular Weight:209.245
Hs Code.:

Synonyms:(2S)-2-hydroxy-N-methoxy-N-methyl-3-phenylpropanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-2-hydroxy-N-methoxy-N-methyl-3-phenylpropanamide

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Technology Process of (2S)-2-hydroxy-N-methoxy-N-methyl-3-phenylpropanamide

There total 7 articles about (2S)-2-hydroxy-N-methoxy-N-methyl-3-phenylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 20312-36-1
L-3-phenyllactic acid

: 1117-97-1
N,0-dimethylhydroxylamine

: 188295-04-7
(2S)-2-hydroxy-N-methoxy-N-methyl-3-phenylpropanamide

Guidance literature:: With C₁₂H₆B₂Br₄O₃; In 1,2-dichloro-ethane; at 90 ℃; for 4h; Reagent/catalyst;
DOI:10.1039/d0cc05630h

Reference yield: 83.0%

: 20312-36-1
L-3-phenyllactic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 188295-04-7
(2S)-2-hydroxy-N-methoxy-N-methyl-3-phenylpropanamide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With 4-methyl-morpholine; In dichloromethane; at 0 ℃; for 0.0833333h; Inert atmosphere;

L-3-phenyllactic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 14.3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2020.152526

Reference yield: 83.0%

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 13673-95-5
(S)-methyl 2-hydroxy-3-phenylpropanoate

: 188295-04-7
(2S)-2-hydroxy-N-methoxy-N-methyl-3-phenylpropanamide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With trimethylaluminum; In tetrahydrofuran; toluene; at 20 ℃; for 0.5h;

(S)-methyl 2-hydroxy-3-phenylpropanoate; In tetrahydrofuran; toluene; at 0 - 80 ℃; for 15.5h;
DOI:10.1021/ja061010o