methyl 3-(butylamino)-2,5-dihydro-2-oxo-1-phenyl-1H-pyrrole-4-carboxylate

Base Information

Chemical Name:methyl 3-(butylamino)-2,5-dihydro-2-oxo-1-phenyl-1H-pyrrole-4-carboxylate
CAS No.:1374118-95-2
Molecular Formula:C₁₆H₂₀N₂O₃
Molecular Weight:288.346
Hs Code.:

Synonyms:methyl 3-(butylamino)-2,5-dihydro-2-oxo-1-phenyl-1H-pyrrole-4-carboxylate

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Chemical Property of methyl 3-(butylamino)-2,5-dihydro-2-oxo-1-phenyl-1H-pyrrole-4-carboxylate

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Technology Process of methyl 3-(butylamino)-2,5-dihydro-2-oxo-1-phenyl-1H-pyrrole-4-carboxylate

There total 3 articles about methyl 3-(butylamino)-2,5-dihydro-2-oxo-1-phenyl-1H-pyrrole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 109-73-9,85404-21-3
N-butylamine

: 62-53-3
aniline

: 762-42-5
dimethyl acetylenedicarboxylate

: 1374118-95-2
methyl 3-(butylamino)-2,5-dihydro-2-oxo-1-phenyl-1H-pyrrole-4-carboxylate

Guidance literature:: With saccharin; In methanol; at 20 ℃; for 4h; Green chemistry;
DOI:10.1007/s13738-016-0871-5

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: C₁₀H₁₇NO₄

: 62-53-3
aniline

: 1374118-95-2
methyl 3-(butylamino)-2,5-dihydro-2-oxo-1-phenyl-1H-pyrrole-4-carboxylate

Guidance literature:: With oxalic acid; In methanol; at 20 ℃; for 3h;
DOI:10.3184/174751912X13547952669204

Reference yield:

: 762-42-5
dimethyl acetylenedicarboxylate

: 1374118-95-2
methyl 3-(butylamino)-2,5-dihydro-2-oxo-1-phenyl-1H-pyrrole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 0.5 h

2: oxalic acid / methanol / 3 h / 20 °C

With oxalic acid; In methanol;
DOI:10.3184/174751912X13547952669204