2-Methyl-selenobenzoic acid Se-ethyl ester

Base Information

Chemical Name:2-Methyl-selenobenzoic acid Se-ethyl ester
CAS No.:135250-01-0
Molecular Formula:C₁₀H₁₂OSe
Molecular Weight:227.165
Hs Code.:

Synonyms:2-Methyl-selenobenzoic acid Se-ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methyl-selenobenzoic acid Se-ethyl ester

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Technology Process of 2-Methyl-selenobenzoic acid Se-ethyl ester

There total 2 articles about 2-Methyl-selenobenzoic acid Se-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 135249-92-2
sodium 2-methylbenzenecarboselenoate

: 75-03-6
ethyl iodide

: 135250-01-0
2-Methyl-selenobenzoic acid Se-ethyl ester

Guidance literature:: at 20 ℃;

Reference yield:

: 933-88-0
ortho-toluoyl chloride

: 135250-01-0
2-Methyl-selenobenzoic acid Se-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium selenide / diethyl ether / 3 h / 22 °C

2: 89 percent / 20 °C

With sodium selenide; In diethyl ether;

Reference yield: 59.0%

: 90-14-2
1-Iodonaphthalene

: 135250-01-0
2-Methyl-selenobenzoic acid Se-ethyl ester

: (1-(ethylselanyl)naphthalen-2-yl)(o-tolyl)methanone

Guidance literature:: With trifuran-2-yl-phosphane; norbornene; potassium carbonate; palladium dichloride; at 100 ℃; for 16h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.8b00112