Technology Process of tert-butyl 4-((phenylthio)carbonyl)butylbenzylcarbamate
There total 7 articles about tert-butyl 4-((phenylthio)carbonyl)butylbenzylcarbamate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
2: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C
3: sodium dihydrogen phosphate monohydrate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h / 0 - 20 °C
4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 - 20 °C
With
dmap; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; sodium chlorite; tetrabutyl ammonium fluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1246/cl.2011.959
- Guidance literature:
-
Multi-step reaction with 7 steps
1: triethylamine / dichloromethane / 3 h / 20 °C
2: 1H-imidazole / dichloromethane / 2 h / 20 °C
3: sodium hydride / tetrahydrofuran / 8 h / 0 - 20 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
5: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C
6: sodium dihydrogen phosphate monohydrate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h / 0 - 20 °C
7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 - 20 °C
With
1H-imidazole; dmap; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; sodium chlorite; tetrabutyl ammonium fluoride; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1246/cl.2011.959
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1H-imidazole / dichloromethane / 2 h / 20 °C
2: sodium hydride / tetrahydrofuran / 8 h / 0 - 20 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C
4: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C
5: sodium dihydrogen phosphate monohydrate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h / 0 - 20 °C
6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 0 - 20 °C
With
1H-imidazole; dmap; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; sodium chlorite; tetrabutyl ammonium fluoride; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; pyridinium chlorochromate;
In
tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1246/cl.2011.959
