C₁₀H₁₀Br₂O₂C₆H₄

Base Information

Chemical Name:C₁₀H₁₀Br₂O₂C₆H₄
CAS No.:937795-32-9
Molecular Formula:C₁₆H₁₄Br₂O₂
Molecular Weight:398.094
Hs Code.:

C<sub>10</sub>H<sub>10</sub>Br<sub>2</sub>O<sub>2</sub>C<sub>6</sub>H<sub>4</sub>

Synonyms:C₁₀H₁₀Br₂O₂C₆H₄

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Chemical Property of C₁₀H₁₀Br₂O₂C₆H₄

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Technology Process of C₁₀H₁₀Br₂O₂C₆H₄

There total 4 articles about C₁₀H₁₀Br₂O₂C₆H₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 937795-30-7
(3,5-dibromophenyl)glycidol

: 100-39-0
benzyl bromide

: 937795-32-9
C₁₀H₁₀Br₂O₂C₆H₄

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at -20 - 20 ℃;
DOI:10.1021/jo062612t

Reference yield:

: 352288-41-6
ethyl 3-(3,5-dibromophenyl)propenopate

: 937795-32-9
C₁₀H₁₀Br₂O₂C₆H₄

Guidance literature:: Multi-step reaction with 3 steps

1: DIBALH / diethyl ether; toluene / 1 h / 0 - 20 °C

2: L-DIPT; Ti(O-i-Pr)4; tert-butyl hydroperoxide / CH₂Cl₂; 2,2,4-trimethyl-pentane / 3 h / -20 °C

3: 93 percent / NaH / dimethylformamide / -20 - 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; sodium hydride; diisobutylaluminium hydride; In 2,2,4-trimethylpentane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene; 2: Sharpless epoxidation;
DOI:10.1021/jo062612t

Reference yield:

: 352288-51-8
3-(3,5-dibromophenyl)prop-2-en-1-ol

: 937795-32-9
C₁₀H₁₀Br₂O₂C₆H₄

Guidance literature:: Multi-step reaction with 2 steps

1: L-DIPT; Ti(O-i-Pr)4; tert-butyl hydroperoxide / CH₂Cl₂; 2,2,4-trimethyl-pentane / 3 h / -20 °C

2: 93 percent / NaH / dimethylformamide / -20 - 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; sodium hydride; In 2,2,4-trimethylpentane; dichloromethane; N,N-dimethyl-formamide; 1: Sharpless epoxidation;
DOI:10.1021/jo062612t