C₂₄H₃₁N₅O₄

Base Information

Chemical Name:C₂₄H₃₁N₅O₄
CAS No.:1246520-20-6
Molecular Formula:C₂₄H₃₁N₅O₄
Molecular Weight:453.541
Hs Code.:

C<sub>24</sub>H<sub>31</sub>N<sub>5</sub>O<sub>4</sub>

Synonyms:C₂₄H₃₁N₅O₄

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Chemical Property of C₂₄H₃₁N₅O₄

Chemical Property:

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Technology Process of C₂₄H₃₁N₅O₄

There total 13 articles about C₂₄H₃₁N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1246521-39-0
C₉H₁₃NO₅

: C₁₉H₂₃N₅O₂*2ClH

: 1246520-20-6
C₂₄H₃₁N₅O₄

Guidance literature:: C₁₉H₂₃N₅O₂*2ClH; With triethylamine; In chloroform; for 0.0833333h; Cooling with ice;

C₉H₁₃NO₅; In chloroform; for 2h; Cooling with ice;

Reference yield:

: 36404-88-3
2-chloro-3-carbaldehydepyridine

: 1246520-20-6
C₂₄H₃₁N₅O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene-4-sulfonic acid; hydrazine hydrate / 21 h / 120 °C / Cooling with ice

2.1: potassium hydroxide; iodine / N,N-dimethyl-formamide / 1 h / 20 °C / Cooling with ice

3.1: sodium hydride / N,N-dimethyl-formamide / 3 h / Cooling with ice

3.2: 1 h / 20 °C / Cooling with ice

4.1: triethylamine / triphenylphosphine; palladium diacetate / 1,4-dioxane / 4 h / 100 °C / Inert atmosphere

5.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 2 h / 20 °C / Cooling with ice

5.2: Cooling with ice

6.1: trifluoroacetic acid / 16 h / Reflux

7.1: hydrogen / palladium 10% on activated carbon / water; tetrahydrofuran; methanol / 3 h / 20 °C

8.1: N-chloro-succinimide; triphenylphosphine / tetrahydrofuran / 0.03 h / 20 °C

8.2: Reflux

9.1: hydrogenchloride; methanol / ethyl acetate; chloroform / 28 h / 20 °C

10.1: triethylamine / chloroform / 0.08 h / Cooling with ice

10.2: 2 h / Cooling with ice

With hydrogenchloride; methanol; N-chloro-succinimide; water; hydrogen; iodine; sodium hydride; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine; triphenylphosphine; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; chloroform; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1070436-97-3
3-iodo-1-(4-methoxybenzyl)-1H-pyrazolo[3,4-b]pyridine

: 1246520-20-6
C₂₄H₃₁N₅O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / triphenylphosphine; palladium diacetate / 1,4-dioxane / 4 h / 100 °C / Inert atmosphere

2.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 2 h / 20 °C / Cooling with ice

2.2: Cooling with ice

3.1: trifluoroacetic acid / 16 h / Reflux

4.1: hydrogen / palladium 10% on activated carbon / water; tetrahydrofuran; methanol / 3 h / 20 °C

5.1: N-chloro-succinimide; triphenylphosphine / tetrahydrofuran / 0.03 h / 20 °C

5.2: Reflux

6.1: hydrogenchloride; methanol / ethyl acetate; chloroform / 28 h / 20 °C

7.1: triethylamine / chloroform / 0.08 h / Cooling with ice

7.2: 2 h / Cooling with ice

With hydrogenchloride; methanol; N-chloro-succinimide; water; hydrogen; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; chloroform; water; ethyl acetate;