2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Base Information

Chemical Name:2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate
CAS No.:848034-59-3
Molecular Formula:C₃₇H₂₉Cl₃O₁₁
Molecular Weight:755.99
Hs Code.:

Synonyms:2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

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Chemical Property of 2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

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Technology Process of 2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

There total 2 articles about 2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 848034-51-5
(2R,3R,4S,5R,6R)-3,4,5-tris(benzoyloxy)-6-((benzoyloxy)methyl)tetrahydro-2H-pyran-2-carboxylic acid

: 115-20-8
1,1,1-trichloroethanol

: 848034-59-3
2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetasy.2004.11.064

Reference yield:

: 286369-06-0
2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonamide

: 848034-59-3
2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / nitrogen(IV) oxide / CH₂Cl₂ / 20 °C

2: 76 percent / 1,3-dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 20 °C

With dmap; Nitrogen dioxide; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tetasy.2004.11.064

Reference yield: 59.0%

: 848034-59-3
2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate

: 2,2,2-trichloroethyl 3,4,5,7-tetra-O-benzoyl-α-D-gluco-hept-2-ulopyranosonate

: 2,2,2-trichloroethyl 2-azido-3,4,5,7-tetra-O-benzoyl-2-deoxy-β-D-gluco-hept-2-ulopyranosonate

Guidance literature:: 2,2,2-trichloroethyl 2,6-anhydro-3,4,5,7-tetra-O-benzoyl-D-glycero-D-gulo-heptonate; With potassium bromate; sodium dithionite; In dichloromethane; water; at 20 ℃;

With sodium azide; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1016/j.tetasy.2004.11.064