ETHYL 2-CARBOXYPYRIDINE-3-CARBOXYLATE

Base Information

• Chemical Name: ETHYL 2-CARBOXYPYRIDINE-3-CARBOXYLATE
• CAS No.: 24195-02-6
• Molecular Formula: C8H7NO4
• Molecular Weight: 181.148
• Hs Code.: 2933399090
• Mol file: 24195-02-6.mol

Synonyms:3-methyl-2-carboxypyridine-3-carboxylate;methyl 2-carboxypyridine-3-carboxylate;2,3-Pyridinedicarboxylic acid, 3-methyl ester;F1936-0002;methyl 2-carboxynicotinate;pyridine-2,3-dicarboxylic acid 3-methyl ester;2,3-pyridinedicarboxylic acid 3-methyl ester;Pyridin-2,3-dicarbonsaeure-3-methylester;

Chemical Property of ETHYL 2-CARBOXYPYRIDINE-3-CARBOXYLATE

Chemical Property:

• Vapor Pressure: 2.41E-05mmHg at 25°C
• Melting Point: 106℃
• Boiling Point: 345°Cat760mmHg
• Flash Point: 162.4°C
• PSA: 76.49000
• Density: 1.361g/cm³
• LogP: 0.56640

Purity/Quality:

97% ^*data from raw suppliers

3-(Methoxycarbonyl)pyridine-2-carboxylicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 2-CARBOXYPYRIDINE-3-CARBOXYLATE

There total 7 articles about ETHYL 2-CARBOXYPYRIDINE-3-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Pyridine-2,3-dicarboxylic anhydride (699-98-9) → pyridine-2,3-dicarboxylic acid 2-methyl ester (24195-07-1) + pyridine-2,3-dicarboxylic acid 3-methyl ester (24195-02-6)

Guidance literature:

In methanol; for 1h; Heating / reflux;

Reference yield:

methanol (67-56-1) + Pyridine-2,3-dicarboxylic anhydride (699-98-9) → pyridine-2,3-dicarboxylic acid 2-methyl ester (24195-07-1) + pyridine-2,3-dicarboxylic acid 3-methyl ester (24195-02-6)

Guidance literature:

DOI:10.1039/jr9570002531 DOI:10.1021/ja01259a070

Reference yield:

Pyridine-2,3-dicarboxylic acid (89-00-9) → pyridine-2,3-dicarboxylic acid 3-methyl ester (24195-02-6)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic anhydride / 4 h / Heating

2: 24 h / 45 °C

With acetic anhydride;

DOI:10.1023/A:1015635303954

upstream raw materials:

methanol

Pyridine-2,3-dicarboxylic anhydride

dimethyl 2,3-pyridinedicarboxylate

Pyridine-2,3-dicarboxylic acid

Downstream raw materials:

pyridine-2,3-dicarboxylic acid 2-methyl ester

methyl 3-pyridinecarboxylate

methyl 3-{[(tert-butoxy)carbonyl]amino}pyridine-2-carboxylate

2-tert-butoxycarbonylamino-nicotinic acid methyl ester

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