[(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]BF4

Base Information

Chemical Name:[(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]BF4
CAS No.:308849-35-6
Molecular Formula:BF₄*C₃₄H₃₆ClIrNP₂
Molecular Weight:835.092
Hs Code.:

Synonyms:[(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]BF4

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Chemical Property of [(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]BF4

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Technology Process of [(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]BF4

There total 1 articles about [(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]BF4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 14104-20-2
silver tetrafluoroborate

: 12354-84-6,12354-85-7
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]

: 2960-37-4
Bis(diphenylphosphanyl)amine

: 308849-35-6
[(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]BF4

Guidance literature:: In chloroform; acetone; (N2); recrystn. (CH2Cl2-Et2O); elem. anal.;
DOI:10.1016/S0022-328X(00)00088-7

Reference yield: 91.0%

: 308849-35-6
[(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]BF4

: [(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]

Guidance literature:: With potassium tert-butoxide; In dichloromethane; toluene; under N2; a mixt. of complex and tert-BuOK in CH2Cl2 was stirred at roomtemp. for 1 h; evapn. of soln., extn. with toluene, evapn. to small vol., cooled to -20°C; elem. anal.;
DOI:10.1016/S0022-328X(02)02036-3

Reference yield: 60.0%

: 308849-35-6
[(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)amine)]BF4

: 74-88-4
methyl iodide

: 519184-40-8
[(η5-pentamethylcyclopentadienyl)IrCl(η2-P,P'-bis(diphenylphosphino)methylamine)]I

Guidance literature:: With potassium tert-butoxide; In dichloromethane; under N2; a mixt. of complex and KC(CH3)3O in dry CH2Cl2 was stirred at room temp. for 1 h; the soln. was evapd. to dryness and solid residue extd. (C6H5CH3); to this solution CH3I was added and the mixt. was heated under reflux for 1 h; filtered, washed with Et2O and under vac.; elem. anal.;
DOI:10.1016/S0022-328X(02)02036-3