D-myo-Inositol, 2,5,6-tris-O-(phenylmethyl)-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene-

Base Information

Chemical Name:D-myo-Inositol, 2,5,6-tris-O-(phenylmethyl)-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene-
CAS No.:196302-90-6
Molecular Formula:C₃₇H₄₄O₆
Molecular Weight:584.753
Hs Code.:

Synonyms:1D-2,5,6-tri-O-benzyl-3-O-endo,4-O-exo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

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Chemical Property of D-myo-Inositol, 2,5,6-tris-O-(phenylmethyl)-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene-

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Technology Process of D-myo-Inositol, 2,5,6-tris-O-(phenylmethyl)-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene-

There total 1 articles about D-myo-Inositol, 2,5,6-tris-O-(phenylmethyl)-3,4-O-(1S,2R,4S)-1,7,7-trimethylbicyclo2.2.1hept-2-ylidene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128525-51-9
(-)-camphor dimethyl acetal

: 196306-65-7,226889-35-6,226889-37-8,226889-38-9
C₃₇H₄₄O₆

: 196306-65-7,226889-35-6,226889-37-8,226889-38-9
1D-2,4,5-tri-O-benzyl-1-O-endo,6-O-exo-(D-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

: 196302-90-6,196306-65-7,226889-35-6,226889-37-8,226889-38-9
1D-2,5,6-tri-O-benzyl-3-O-endo,4-O-exo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

: 196306-65-7,226889-35-6,226889-37-8,226889-38-9
1D-2,4,5-tri-O-benzyl-1-O-exo,6-O-endo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

: 196306-65-7,226889-35-6,226889-37-8,226889-38-9
1D-2,5,6-tri-O-benzyl-3-O-exo,4-O-endo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

Guidance literature:: With toluene-4-sulfonic acid; Yield given; Multistep reaction. Title compound not separated from byproducts; 1.) MeOH, overnight, 2.) CH₂Cl₂, reflux, 2 h;

Reference yield: 98.0%

: 824-94-2
p-methoxybenzyl chloride

: 196302-90-6,196306-65-7,226889-35-6,226889-37-8,226889-38-9
1D-2,5,6-tri-O-benzyl-3-O-endo,4-O-exo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

: 196302-91-7
C₄₅H₅₂O₇

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;

Reference yield:

: 196302-90-6,196306-65-7,226889-35-6,226889-37-8,226889-38-9
1D-2,5,6-tri-O-benzyl-3-O-endo,4-O-exo-(L-1',7',7'-trimethylbicyclo<2.2.1>hept-2'-ylidene)-myo-inositol

: 141040-54-2
(+)-2,5,6-tri-O-benzyl-1-O-(p-methoxybenzyl)-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaH / dimethylformamide / 0 - 20 °C

2: AcCl, MeOH / CH₂Cl₂

With methanol; sodium hydride; acetyl chloride; In dichloromethane; N,N-dimethyl-formamide;