Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

Base Information

Chemical Name:Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone
CAS No.:182310-69-6
Molecular Formula:C₆₅H₈₂O₇
Molecular Weight:975.362
Hs Code.:

Synonyms:Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

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Chemical Property of Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

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Technology Process of Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

There total 4 articles about Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 98-54-4
para-tert-butylphenol

: 182310-66-3
Bis-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-phenyl]-methanone

: 182310-69-6
Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Heating;
DOI:10.1016/0040-4039(96)01287-7

Reference yield:

: 25446-98-4
2,2'-dihydroxy-5,5'-di-tert-butylbenzophenone

: 182310-69-6
Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / HCl, H₃PO₄ / acetic acid / 100 °C

2: 80 percent / p-TsOH / benzene / Heating

3: 34 percent / 20percent NaOH (aq.) / methanol / 60 °C

4: 59 percent / p-TsOH / benzene / Heating

With hydrogenchloride; sodium hydroxide; phosphoric acid; toluene-4-sulfonic acid; In methanol; acetic acid; benzene;
DOI:10.1016/0040-4039(96)01287-7

Reference yield:

: 149826-78-8
4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol

: 182310-69-6
Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / p-TsOH / benzene / Heating

2: 34 percent / 20percent NaOH (aq.) / methanol / 60 °C

3: 59 percent / p-TsOH / benzene / Heating

With sodium hydroxide; toluene-4-sulfonic acid; In methanol; benzene;
DOI:10.1016/0040-4039(96)01287-7