{5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

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Chemical Name:{5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone
CAS No.:182310-73-2
Molecular Formula:C₆₆H₈₄O₈
Molecular Weight:1005.39
Hs Code.:

{5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

Synonyms:{5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

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Chemical Property of {5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

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Technology Process of {5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

There total 5 articles about {5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 182310-69-6
Bis-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

: 182310-73-2
{5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; at 60 ℃;
DOI:10.1016/0040-4039(96)01287-7

Reference yield:

: 25446-98-4
2,2'-dihydroxy-5,5'-di-tert-butylbenzophenone

: 182310-73-2
{5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / HCl, H₃PO₄ / acetic acid / 100 °C

2: 80 percent / p-TsOH / benzene / Heating

3: 34 percent / 20percent NaOH (aq.) / methanol / 60 °C

4: 59 percent / p-TsOH / benzene / Heating

5: 52 percent / 20percent NaOH (aq.) / dioxane / 60 °C

With hydrogenchloride; sodium hydroxide; phosphoric acid; toluene-4-sulfonic acid; In 1,4-dioxane; methanol; acetic acid; benzene;
DOI:10.1016/0040-4039(96)01287-7

Reference yield:

: 149790-91-0
4-t-butyl-2-<5-t-butyl-3-<5-t-butyl-3-(5-t-butylsalicyl)salicyloyl>salicyl>phenol

: 182310-73-2
{5-tert-Butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-{5-tert-butyl-3-[5-tert-butyl-3-(5-tert-butyl-2-hydroxy-3-hydroxymethyl-benzyl)-2-hydroxy-benzyl]-2-hydroxy-phenyl}-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: 34 percent / 20percent NaOH (aq.) / methanol / 60 °C

2: 59 percent / p-TsOH / benzene / Heating

3: 52 percent / 20percent NaOH (aq.) / dioxane / 60 °C

With sodium hydroxide; toluene-4-sulfonic acid; In 1,4-dioxane; methanol; benzene;
DOI:10.1016/0040-4039(96)01287-7