4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol

Base Information

Chemical Name:4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol
CAS No.:149826-78-8
Molecular Formula:C₂₃H₂₈Cl₂O₃
Molecular Weight:423.38
Hs Code.:

Synonyms:4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol

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Chemical Property of 4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol

Chemical Property:

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Technology Process of 4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol

There total 4 articles about 4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 25446-98-4
2,2'-dihydroxy-5,5'-di-tert-butylbenzophenone

: 149826-78-8
4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol

Guidance literature:: With hydrogenchloride; phosphoric acid; acetic acid; at 80 ℃; for 10h;
DOI:10.1246/bcsj.66.828

Reference yield:

: 799-13-3
bis(5-tert-butyl-2-hydroxyphenyl)methane

: 149826-78-8
4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol

Guidance literature:: Multi-step reaction with 4 steps

1: aq. HCl / 4 h / 100 °C

2: 65 percent / aq. CrO₃, acetic anhydride / 1 h / 60 °C

3: 10percent aq. NaOH / methanol / 8 h / 50 °C

4: 89 percent / H₃PO₄, AcOH, aq. HCl / 10 h / 80 °C

With chromium(VI) oxide; hydrogenchloride; sodium hydroxide; phosphoric acid; acetic anhydride; acetic acid; In methanol;
DOI:10.1246/bcsj.66.828

Reference yield:

: 149790-47-6
Acetic acid 2-(2-acetoxy-5-tert-butyl-benzyl)-4-tert-butyl-phenyl ester

: 149826-78-8
4-t-butyl-2-(5-t-butyl-3-chloromethylsalicyloyl)-6-chloromethylphenol

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / aq. CrO₃, acetic anhydride / 1 h / 60 °C

2: 10percent aq. NaOH / methanol / 8 h / 50 °C

3: 89 percent / H₃PO₄, AcOH, aq. HCl / 10 h / 80 °C

With chromium(VI) oxide; hydrogenchloride; sodium hydroxide; phosphoric acid; acetic anhydride; acetic acid; In methanol;
DOI:10.1246/bcsj.66.828