(E)-2-Phenyl-ethenesulfonic acid methyl-[2-(phenyl-hydrazono)-ethyl]-amide

Base Information

Chemical Name:(E)-2-Phenyl-ethenesulfonic acid methyl-[2-(phenyl-hydrazono)-ethyl]-amide
CAS No.:198694-08-5
Molecular Formula:C₁₇H₁₉N₃O₂S
Molecular Weight:329.423
Hs Code.:

Synonyms:(E)-2-Phenyl-ethenesulfonic acid methyl-[2-(phenyl-hydrazono)-ethyl]-amide

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Chemical Property of (E)-2-Phenyl-ethenesulfonic acid methyl-[2-(phenyl-hydrazono)-ethyl]-amide

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Technology Process of (E)-2-Phenyl-ethenesulfonic acid methyl-[2-(phenyl-hydrazono)-ethyl]-amide

There total 3 articles about (E)-2-Phenyl-ethenesulfonic acid methyl-[2-(phenyl-hydrazono)-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 100-63-0
phenylhydrazine

: 198694-03-0
(E)-2-Phenyl-ethenesulfonic acid methyl-(2-oxo-ethyl)-amide

: 198694-08-5
(E)-2-Phenyl-ethenesulfonic acid methyl-[2-(phenyl-hydrazono)-ethyl]-amide

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; at 0 ℃; for 6h;
DOI:10.1016/S0040-4020(97)00874-0

Reference yield:

: 52147-97-4
trans 2-phenylethenesulfonyl chloride

: 198694-08-5
(E)-2-Phenyl-ethenesulfonic acid methyl-[2-(phenyl-hydrazono)-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Et₃N / CCl₄ / 6 h / 25 °C

2: 82 percent / PPTS / H₂O; acetone / Heating

3: 91 percent / p-TsOH / aq. ethanol / 6 h / 0 °C

With pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; triethylamine; In tetrachloromethane; ethanol; water; acetone;
DOI:10.1016/S0040-4020(97)00874-0

Reference yield:

: 198694-02-9
(E)-2-Phenyl-ethenesulfonic acid (2,2-dimethoxy-ethyl)-methyl-amide

: 198694-08-5
(E)-2-Phenyl-ethenesulfonic acid methyl-[2-(phenyl-hydrazono)-ethyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / PPTS / H₂O; acetone / Heating

2: 91 percent / p-TsOH / aq. ethanol / 6 h / 0 °C

With pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; In ethanol; water; acetone;
DOI:10.1016/S0040-4020(97)00874-0