[Zn(2,2'-(2,2'-bipyridine-6,6'-diyl)bis(1,1-diphenylethanethiolate(-2H))]

Base Information

Chemical Name:[Zn(2,2'-(2,2'-bipyridine-6,6'-diyl)bis(1,1-diphenylethanethiolate(-2H))]
CAS No.:1335107-86-2
Molecular Formula:C₃₈H₃₀N₂S₂Zn
Molecular Weight:644.192
Hs Code.:

Synonyms:[Zn(2,2'-(2,2'-bipyridine-6,6'-diyl)bis(1,1-diphenylethanethiolate(-2H))]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Zn(2,2'-(2,2'-bipyridine-6,6'-diyl)bis(1,1-diphenylethanethiolate(-2H))]

Chemical Property:

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Technology Process of [Zn(2,2'-(2,2'-bipyridine-6,6'-diyl)bis(1,1-diphenylethanethiolate(-2H))]

There total 1 articles about [Zn(2,2'-(2,2'-bipyridine-6,6'-diyl)bis(1,1-diphenylethanethiolate(-2H))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 557-34-6
zinc diacetate

: 203871-22-1
2,2’-(2,2’-bipyridine-6,6’-diyl)bis(1,1’-diphenylethanethiolate)

: 1335107-86-2
[Zn(2,2'-(2,2'-bipyridine-6,6'-diyl)bis(1,1-diphenylethanethiolate(-2H))]

Guidance literature:: With NaH; In tetrahydrofuran; methanol; (Ar); Schlenk technique; NaH was added to soln. of ligand in THF; after 20 min filtered; soln. of zn salt in MeOH/THF (1/4) was added; reacted for 1 h; evapd. (vac.); extd. (CH2Cl2); evapd. (vac.); washed (MeOH); recrystd. (CH2Cl2/MeOH, 2/1); elem. anal.;
DOI:10.1021/ic200899w

Reference yield:

: 1335107-86-2
[Zn(2,2'-(2,2'-bipyridine-6,6'-diyl)bis(1,1-diphenylethanethiolate(-2H))]

: 74-88-4
methyl iodide

: 1335107-88-4
[ZnI₂((NC₅H₃CH₂C(C₆H₅)2SCH₃)2)]

Guidance literature:: In dichloromethane; (Ar); Schlenk technique; soln. of Zn complex in CH2Cl2 was treated with MeI (20 equiv.); Kinetics;
DOI:10.1021/ic200899w