Mo₂Fe₇S₈(SCH₂CH₃)12^(3-)*3(CH₃)3NCH₂C₆H₅⁽¹⁺⁾={(CH₃)3NCH₂C₆H₅}3Mo₂Fe₇S₈(SCH₂CH₃)12

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• Chemical Name: Mo₂Fe₇S₈(SCH₂CH₃)12^(3-)*3(CH₃)3NCH₂C₆H₅⁽¹⁺⁾={(CH₃)3NCH₂C₆H₅}3Mo₂Fe₇S₈(SCH₂CH₃)12
• CAS No.: 72268-97-4
• Molecular Formula: 3C₁₀H₁₆N*C₂₄H₆₀Fe₇Mo₂S₂₀
• Molecular Weight: 2023.6

Synonyms:Mo₂Fe₇S₈(SCH₂CH₃)12^(3-)*3(CH₃)3NCH₂C₆H₅⁽¹⁺⁾={(CH₃)3NCH₂C₆H₅}3Mo₂Fe₇S₈(SCH₂CH₃)12

Chemical Property of Mo₂Fe₇S₈(SCH₂CH₃)12^(3-)*3(CH₃)3NCH₂C₆H₅⁽¹⁺⁾={(CH₃)3NCH₂C₆H₅}3Mo₂Fe₇S₈(SCH₂CH₃)12

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Technology Process of Mo₂Fe₇S₈(SCH₂CH₃)12^(3-)*3(CH₃)3NCH₂C₆H₅⁽¹⁺⁾={(CH₃)3NCH₂C₆H₅}3Mo₂Fe₇S₈(SCH₂CH₃)12

There total 1 articles about Mo₂Fe₇S₈(SCH₂CH₃)12^(3-)*3(CH₃)3NCH₂C₆H₅⁽¹⁺⁾={(CH₃)3NCH₂C₆H₅}3Mo₂Fe₇S₈(SCH₂CH₃)12 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

benzyltrimethylammonium tetrathiomolybdate + iron(III) chloride (7705-08-0) + ethanethiol (75-08-1) → Mo2Fe7S8(SCH2CH3)12(3-)*3(CH3)3NCH2C6H5(1+)={(CH3)3NCH2C6H5}3Mo2Fe7S8(SCH2CH3)12 (72268-97-4)

Guidance literature:

With NaOCH₃; In methanol; (N2), soln. of ethanethiol and NaOCH3 in methanol added to filtered soln. of FeCl3 in methanol, slurry of (Me3NCH2Ph)2MoS4 in methanol added, stirred overnight; filtered, washed with ethanol, dried in vacuo, residue extracted with warm CH3CN (50°C), extract filtered, volume reduced, cooled to -20°C, recrystd. from CH3CN, elem. anal.;

DOI:10.1021/ja00534a023

Reference yield: 62.0%

Mo2Fe7S8(SCH2CH3)12(3-)*3(CH3)3NCH2C6H5(1+)={(CH3)3NCH2C6H5}3Mo2Fe7S8(SCH2CH3)12 (72268-97-4) + acetyl chloride (75-36-5) → Mo2Fe7S8(SCH2CH3)6Cl6(3-)*3(CH3)3NCH2C6H5(1+)={(CH3)3NCH2C6H5}3Mo2Fe7S8(SCH2CH3)6Cl6 (79466-67-4)

Guidance literature:

In acetonitrile; 50°C, 90 min, volume was reduced; addn. of THF, storage at -15°C overnight, solid was collected and washed with THF/acetonitrile, elem. anal.;

upstream raw materials:

iron(III) chloride

ethanethiol

Downstream raw materials:

Mo₂Fe₇S₈(SCH₂CH₃)6Cl₆^(3-)*3(CH₃)3NCH₂C₆H₅⁽¹⁺⁾={(CH₃)3NCH₂C₆H₅}3Mo₂Fe₇S₈(SCH₂CH₃)6Cl₆

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