(3-tert-butoxycarbonylamino-5-formyl-phenyl)-carbamic acid tert-butyl ester

Base Information

Chemical Name:(3-tert-butoxycarbonylamino-5-formyl-phenyl)-carbamic acid tert-butyl ester
CAS No.:364038-89-1
Molecular Formula:C₁₇H₂₄N₂O₅
Molecular Weight:336.388
Hs Code.:

Synonyms:(3-tert-butoxycarbonylamino-5-formyl-phenyl)-carbamic acid tert-butyl ester

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Chemical Property of (3-tert-butoxycarbonylamino-5-formyl-phenyl)-carbamic acid tert-butyl ester

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Technology Process of (3-tert-butoxycarbonylamino-5-formyl-phenyl)-carbamic acid tert-butyl ester

There total 4 articles about (3-tert-butoxycarbonylamino-5-formyl-phenyl)-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 207745-86-6
di-tert-butyl 5-(hydroxymethyl)-1,3-phenylene dicarbamate

: 364038-89-1
(3-tert-butoxycarbonylamino-5-formyl-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: With silica gel; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 28150-13-2
3,5-diaminobenzyl alcohol

: 364038-89-1
(3-tert-butoxycarbonylamino-5-formyl-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-dioxane / 12 h / 20 °C / Alkaline conditions

2: pyridinium chlorochromate; silica gel / dichloromethane / 3 h / 20 °C

With silica gel; pyridinium chlorochromate; In 1,4-dioxane; dichloromethane;

Reference yield:

: 99-34-3
3,5-dinitrobenzoic acid

: 364038-89-1
(3-tert-butoxycarbonylamino-5-formyl-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 12 h / 0 °C / Reflux

2: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 2280.15 Torr / Autoclave

3: 1,4-dioxane / 12 h / 20 °C / Alkaline conditions

4: pyridinium chlorochromate; silica gel / dichloromethane / 3 h / 20 °C

With dimethylsulfide borane complex; palladium 10% on activated carbon; hydrogen; silica gel; pyridinium chlorochromate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;