(5-methoxy-1,2-dimethyl-4,7-dioxoindol-3-yl)methyloxyphenyl-4-phenyl carbonate

Base Information

Chemical Name:(5-methoxy-1,2-dimethyl-4,7-dioxoindol-3-yl)methyloxyphenyl-4-phenyl carbonate
CAS No.:945630-01-3
Molecular Formula:C₂₆H₂₃NO₇
Molecular Weight:461.471
Hs Code.:

Synonyms:(5-methoxy-1,2-dimethyl-4,7-dioxoindol-3-yl)methyloxyphenyl-4-phenyl carbonate

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Chemical Property of (5-methoxy-1,2-dimethyl-4,7-dioxoindol-3-yl)methyloxyphenyl-4-phenyl carbonate

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Technology Process of (5-methoxy-1,2-dimethyl-4,7-dioxoindol-3-yl)methyloxyphenyl-4-phenyl carbonate

There total 4 articles about (5-methoxy-1,2-dimethyl-4,7-dioxoindol-3-yl)methyloxyphenyl-4-phenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 945629-93-6
3-[(4-hydroxymethyl)phenoxy]methyl-5-methoxy-1,2-dimethylindole-4,7-dione

: 1885-14-9
phenyl chloroformate

: 945630-01-3
(5-methoxy-1,2-dimethyl-4,7-dioxoindol-3-yl)methyloxyphenyl-4-phenyl carbonate

Guidance literature:: In pyridine; at 20 ℃;
DOI:10.1039/b703370b

Reference yield:

: 945629-92-5
3-[4-(tert-butyldimethylsiloxymethyl)phenoxymethyl]-5-methoxy-1,2-dimethylindole-4,7-dione

: 945630-01-3
(5-methoxy-1,2-dimethyl-4,7-dioxoindol-3-yl)methyloxyphenyl-4-phenyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

2: 67 percent / pyridine / 20 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran; pyridine;
DOI:10.1039/b703370b

Reference yield:

: 126070-20-0
4-((tert-butyldimethylsilyloxy)methyl)phenol

: 945630-01-3
(5-methoxy-1,2-dimethyl-4,7-dioxoindol-3-yl)methyloxyphenyl-4-phenyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 42 percent / diethyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C

2: 74 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

3: 67 percent / pyridine / 20 °C

With tetrabutyl ammonium fluoride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; pyridine; 1: Mitsunobu reaction;
DOI:10.1039/b703370b