(S)-4-Benzyloxycarbonylamino-6-methyl-3-oxo-2-phenethyl-heptanoic acid allyl ester

Base Information

Chemical Name:(S)-4-Benzyloxycarbonylamino-6-methyl-3-oxo-2-phenethyl-heptanoic acid allyl ester
CAS No.:1026536-76-4
Molecular Formula:C₂₇H₃₃NO₅
Molecular Weight:451.563
Hs Code.:

Synonyms:(S)-4-Benzyloxycarbonylamino-6-methyl-3-oxo-2-phenethyl-heptanoic acid allyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-Benzyloxycarbonylamino-6-methyl-3-oxo-2-phenethyl-heptanoic acid allyl ester

Chemical Property:

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Technology Process of (S)-4-Benzyloxycarbonylamino-6-methyl-3-oxo-2-phenethyl-heptanoic acid allyl ester

There total 3 articles about (S)-4-Benzyloxycarbonylamino-6-methyl-3-oxo-2-phenethyl-heptanoic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54448-36-1
[2-(trifluoromethylsulfonyloxy)ethyl]benzene

: 387866-57-1
4(S)-benzyloxycarbonylamino-6-methyl-3-oxoheptanoic acid allyl ester

: 1026536-76-4
(S)-4-Benzyloxycarbonylamino-6-methyl-3-oxo-2-phenethyl-heptanoic acid allyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/jo010270f

Reference yield:

: 2018-66-8
Z-Leu-OH

: 1026536-76-4
(S)-4-Benzyloxycarbonylamino-6-methyl-3-oxo-2-phenethyl-heptanoic acid allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / carbonyl-1,1'-diimidazole; BuLi; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

2: NaH / tetrahydrofuran / 0 - 20 °C

With n-butyllithium; sodium hydride; diisopropylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran;
DOI:10.1021/jo010270f

Reference yield:

: 591-87-7
Allyl acetate

: 1026536-76-4
(S)-4-Benzyloxycarbonylamino-6-methyl-3-oxo-2-phenethyl-heptanoic acid allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / carbonyl-1,1'-diimidazole; BuLi; diisopropylamine / tetrahydrofuran / 0.5 h / -78 °C

2: NaH / tetrahydrofuran / 0 - 20 °C

With n-butyllithium; sodium hydride; diisopropylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran;
DOI:10.1021/jo010270f