C₅₇H₇₄N₁₀O₄

Base Information

• Chemical Name: C₅₇H₇₄N₁₀O₄
• CAS No.: 152429-67-9
• Molecular Formula: C₅₇H₇₄N₁₀O₄
• Molecular Weight: 963.279
• Mol file: 152429-67-9.mol

Synonyms:C₅₇H₇₄N₁₀O₄

Chemical Property of C₅₇H₇₄N₁₀O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₇H₇₄N₁₀O₄

There total 3 articles about C₅₇H₇₄N₁₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde (100-52-7) → C57H74N10O4 (152429-67-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 2.) NaBH₄ / 1.) benzene, reflux, 6 h, 2.) EtOH, RT, 3 h

2: 32 percent / Et₃N, KI / dimethylformamide / 72 h / Ambient temperature

3: 24 percent / H₂, 3 N HCl / 10percent Pd/C / ethanol / 12 h / 50 °C / 3800 Torr

With hydrogenchloride; sodium tetrahydroborate; hydrogen; triethylamine; potassium iodide; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm00075a032

Reference yield:

N,N'-bis(6-aminohexyl)-N,N'-dimethyl-1,8-octanediamine (115962-75-9) → C57H74N10O4 (152429-67-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 2.) NaBH₄ / 1.) benzene, reflux, 6 h, 2.) EtOH, RT, 3 h

2: 32 percent / Et₃N, KI / dimethylformamide / 72 h / Ambient temperature

3: 24 percent / H₂, 3 N HCl / 10percent Pd/C / ethanol / 12 h / 50 °C / 3800 Torr

With hydrogenchloride; sodium tetrahydroborate; hydrogen; triethylamine; potassium iodide; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm00075a032

Reference yield:

N,N'-Bis-(6-benzylamino-hexyl)-N,N'-dimethyl-octane-1,8-diamine (158094-51-0) → C57H74N10O4 (152429-67-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 32 percent / Et₃N, KI / dimethylformamide / 72 h / Ambient temperature

2: 24 percent / H₂, 3 N HCl / 10percent Pd/C / ethanol / 12 h / 50 °C / 3800 Torr

With hydrogenchloride; hydrogen; triethylamine; potassium iodide; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm00075a032

upstream raw materials:

benzaldehyde

N,N'-bis(6-aminohexyl)-N,N'-dimethyl-1,8-octanediamine

N,N'-Bis-(6-benzylamino-hexyl)-N,N'-dimethyl-octane-1,8-diamine

Downstream raw materials:

C₇₁H₈₃N₁₃O₆

Tripitramine

Refernces