methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

Base Information

Chemical Name:methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate
CAS No.:170997-54-3
Molecular Formula:C₂₄H₃₉NO₈Si
Molecular Weight:497.661
Hs Code.:

Synonyms:methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

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Chemical Property of methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

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Technology Process of methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

There total 2 articles about methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 170997-53-2
methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-D-gluconate

: 170997-54-3
methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 10h; Ambient temperature;

Reference yield:

: 170997-52-1
methyl 2-benzyloxycarbonylamino-2-deoxy-3,4;5,6-di-O-isopropylidene-D-gluconate

: 170997-54-3
methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Dowex 50W-X₈ resin / methanol; H₂O / 52 h / Ambient temperature

2: 94 percent / imidazole / dimethylformamide / 10 h / Ambient temperature

With 1H-imidazole; Dowex 50W-X₈ resin; In methanol; water; N,N-dimethyl-formamide;