methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyloxy-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

Base Information

Chemical Name:methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyloxy-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate
CAS No.:170997-55-4
Molecular Formula:C₂₅H₄₁NO₁₀SSi
Molecular Weight:575.753
Hs Code.:

Synonyms:methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyloxy-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

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Chemical Property of methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyloxy-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

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Technology Process of methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyloxy-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

There total 4 articles about methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyloxy-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 124-63-0
methanesulfonyl chloride

: 170997-54-3
methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

: 170997-55-4
methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyloxy-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 170997-55-4
methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyloxy-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / imidazole / dimethylformamide / 10 h / Ambient temperature

2: 97 percent / Et₃N / tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 170997-53-2
methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-D-gluconate

: 170997-55-4
methyl 2-benzyloxycarbonylamino-2-deoxy-3,4-O-isopropylidene-5-O-methanesulfonyloxy-6-O-(tert-butyldimethylsilyl)oxy-D-gluconate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / imidazole / dimethylformamide / 10 h / Ambient temperature

2: 97 percent / Et₃N / tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;